C₃₀H₂₇BBrF₂IN₂S₂

Base Information

Chemical Name:C₃₀H₂₇BBrF₂IN₂S₂
CAS No.:1588866-88-9
Molecular Formula:C₃₀H₂₇BBrF₂IN₂S₂
Molecular Weight:735.306
Hs Code.:

C<sub>30</sub>H<sub>27</sub>BBrF<sub>2</sub>IN<sub>2</sub>S<sub>2</sub>

Synonyms:C₃₀H₂₇BBrF₂IN₂S₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₀H₂₇BBrF₂IN₂S₂

Chemical Property:

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Technology Process of C₃₀H₂₇BBrF₂IN₂S₂

There total 8 articles about C₃₀H₂₇BBrF₂IN₂S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1588866-87-8
C₃₀H₂₈BBrF₂N₂S₂

: 1588866-88-9
C₃₀H₂₇BBrF₂IN₂S₂

Guidance literature:: With Iodine monochloride; In methanol; dichloromethane; at 60 ℃; for 18h; Reagent/catalyst;
DOI:10.1021/ol500572t

Reference yield:

: 147804-55-5
5-(4-methylphenyl)dipyrromethane

: 1588866-88-9
C₃₀H₂₇BBrF₂IN₂S₂

Guidance literature:: Multi-step reaction with 6 steps

1: chloranil / dichloromethane / 2 h / 20 °C / Inert atmosphere

2: triethylamine; chloranil; boron trifluoride diethyl etherate / dichloromethane / 2 h / 20 °C / Inert atmosphere

3: Iodine monochloride / dichloromethane; methanol / 5 h / 55 °C

4: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; caesium carbonate; tri-tert-butyl phosphine / tetrahydrofuran / 18 h / 35 °C

5: N-Bromosuccinimide / chloroform / 0 °C

6: Iodine monochloride / dichloromethane; methanol / 18 h / 60 °C

With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; N-Bromosuccinimide; tri-tert-butyl phosphine; boron trifluoride diethyl etherate; Iodine monochloride; chloranil; caesium carbonate; triethylamine; In tetrahydrofuran; methanol; dichloromethane; chloroform;
DOI:10.1021/ol500572t

Reference yield:

: 1606994-41-5
5-(4-methylphenyl)dipyrrin

: 1588866-88-9
C₃₀H₂₇BBrF₂IN₂S₂

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine; chloranil; boron trifluoride diethyl etherate / dichloromethane / 2 h / 20 °C / Inert atmosphere

2: Iodine monochloride / dichloromethane; methanol / 5 h / 55 °C

3: tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; caesium carbonate; tri-tert-butyl phosphine / tetrahydrofuran / 18 h / 35 °C

4: N-Bromosuccinimide / chloroform / 0 °C

5: Iodine monochloride / dichloromethane; methanol / 18 h / 60 °C

With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; N-Bromosuccinimide; tri-tert-butyl phosphine; boron trifluoride diethyl etherate; Iodine monochloride; chloranil; caesium carbonate; triethylamine; In tetrahydrofuran; methanol; dichloromethane; chloroform;
DOI:10.1021/ol500572t