3-difluoromethyl-1-methyl-1H-pyrazole-4-carboxylic acid methoxy-[1-(2,2,4-trimethyl-cyclohex-3-enyl)-ethyl]-amide

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Chemical Name:3-difluoromethyl-1-methyl-1H-pyrazole-4-carboxylic acid methoxy-[1-(2,2,4-trimethyl-cyclohex-3-enyl)-ethyl]-amide
CAS No.:1329091-10-2
Molecular Formula:C₁₈H₂₇F₂N₃O₂
Molecular Weight:355.428
Hs Code.:

Synonyms:3-difluoromethyl-1-methyl-1H-pyrazole-4-carboxylic acid methoxy-[1-(2,2,4-trimethyl-cyclohex-3-enyl)-ethyl]-amide

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Chemical Property of 3-difluoromethyl-1-methyl-1H-pyrazole-4-carboxylic acid methoxy-[1-(2,2,4-trimethyl-cyclohex-3-enyl)-ethyl]-amide

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Technology Process of 3-difluoromethyl-1-methyl-1H-pyrazole-4-carboxylic acid methoxy-[1-(2,2,4-trimethyl-cyclohex-3-enyl)-ethyl]-amide

There total 3 articles about 3-difluoromethyl-1-methyl-1H-pyrazole-4-carboxylic acid methoxy-[1-(2,2,4-trimethyl-cyclohex-3-enyl)-ethyl]-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 141573-96-8
3‐difluoromethyl‐1‐methylpyrazole-4-carbonyl chloride

: 1329111-42-3
O-methyl-N-[1-(2,2,4-trimethyl-cyclohex-3-enyl)-ethyl]-hydroxylamine

: 1329091-10-2
3-difluoromethyl-1-methyl-1H-pyrazole-4-carboxylic acid methoxy-[1-(2,2,4-trimethyl-cyclohex-3-enyl)-ethyl]-amide

Guidance literature:: With triethylamine; In dichloromethane; at 24 ℃; for 16h; Product distribution / selectivity; Inert atmosphere;

Reference yield:

: 1000-86-8
2,4-Dimethyl-1,3-pentadiene

: 1329091-10-2
3-difluoromethyl-1-methyl-1H-pyrazole-4-carboxylic acid methoxy-[1-(2,2,4-trimethyl-cyclohex-3-enyl)-ethyl]-amide

Guidance literature:: Multi-step reaction with 4 steps

1.1: aluminum (III) chloride / tetrahydrofuran / 5 - 20 °C

1.2: 19.5 h / 15 - 45 °C

2.1: pyridine / methanol / 16 h / 24 °C / Inert atmosphere

3.1: sodium cyanoborohydride; acetic acid / 16 h / 24 °C / Inert atmosphere

4.1: triethylamine / dichloromethane / 16 h / 24 °C / Inert atmosphere

With pyridine; sodium cyanoborohydride; acetic acid; triethylamine; aluminum (III) chloride; In tetrahydrofuran; methanol; dichloromethane; 1.2: Diels-Alder Reaction;

Reference yield:

: 55695-36-8
1-(3,3,4-trimethyl-cyclohex-3-enyl)-ethanone

: 1329091-10-2
3-difluoromethyl-1-methyl-1H-pyrazole-4-carboxylic acid methoxy-[1-(2,2,4-trimethyl-cyclohex-3-enyl)-ethyl]-amide

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / methanol / 16 h / 24 °C / Inert atmosphere

2: sodium cyanoborohydride; acetic acid / 16 h / 24 °C / Inert atmosphere

3: triethylamine / dichloromethane / 16 h / 24 °C / Inert atmosphere

With pyridine; sodium cyanoborohydride; acetic acid; triethylamine; In methanol; dichloromethane;