methyl 3-O-(2-azidobenzyl)-4,6-O-benzylidene-2-O-p-methoxybenzyl-α-D-glucopyranoside

Base Information

Chemical Name:methyl 3-O-(2-azidobenzyl)-4,6-O-benzylidene-2-O-p-methoxybenzyl-α-D-glucopyranoside
CAS No.:1425503-91-8
Molecular Formula:C₂₉H₃₁N₃O₇
Molecular Weight:533.581
Hs Code.:

Synonyms:methyl 3-O-(2-azidobenzyl)-4,6-O-benzylidene-2-O-p-methoxybenzyl-α-D-glucopyranoside

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Chemical Property of methyl 3-O-(2-azidobenzyl)-4,6-O-benzylidene-2-O-p-methoxybenzyl-α-D-glucopyranoside

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Technology Process of methyl 3-O-(2-azidobenzyl)-4,6-O-benzylidene-2-O-p-methoxybenzyl-α-D-glucopyranoside

There total 1 articles about methyl 3-O-(2-azidobenzyl)-4,6-O-benzylidene-2-O-p-methoxybenzyl-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 31553-17-0
1-azido-2-(bromomethyl)benzene

: methyl 4,6-O-benzylidene-2-O-(p-methoxybenzyl)-α-D-glucopyranoside

: 1425503-91-8
methyl 3-O-(2-azidobenzyl)-4,6-O-benzylidene-2-O-p-methoxybenzyl-α-D-glucopyranoside

Guidance literature:: methyl 4,6-O-benzylidene-2-O-(p-methoxybenzyl)-α-D-glucopyranoside; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h;

1-azido-2-(bromomethyl)benzene; In N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1002/ejoc.201201076

Reference yield:

: 1425503-91-8
methyl 3-O-(2-azidobenzyl)-4,6-O-benzylidene-2-O-p-methoxybenzyl-α-D-glucopyranoside

: 1425503-86-1
C₄₆H₅₁N₃O₁₁S

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine; copper(l) iodide / dichloromethane / 12 h / 20 °C

2: 2,3-dicyano-5,6-dichloro-p-benzoquinone; water / dichloromethane / 2 h / 0 °C

With copper(l) iodide; water; N-ethyl-N,N-diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane;
DOI:10.1002/ejoc.201201076

Reference yield:

: 1425503-91-8
methyl 3-O-(2-azidobenzyl)-4,6-O-benzylidene-2-O-p-methoxybenzyl-α-D-glucopyranoside

: 1425503-87-2
C₄₄H₄₅N₃O₁₁

: C₄₄H₄₅N₃O₁₁

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine; copper(l) iodide / dichloromethane / 12 h / 20 °C

2: 2,3-dicyano-5,6-dichloro-p-benzoquinone; water / dichloromethane / 2 h / 0 °C

3: N-iodo-succinimide; trifluorormethanesulfonic acid / dichloromethane / -40 - 20 °C / Inert atmosphere

With N-iodo-succinimide; copper(l) iodide; trifluorormethanesulfonic acid; water; N-ethyl-N,N-diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane;
DOI:10.1002/ejoc.201201076