5-[α-Carboxy-β-(4'-hydroxy-3',5'-dimethoxyphenyl) ethenyl]-3-methylisoxazole

Base Information

Chemical Name:5-[α-Carboxy-β-(4'-hydroxy-3',5'-dimethoxyphenyl) ethenyl]-3-methylisoxazole
CAS No.:113465-45-5
Molecular Formula:C₁₅H₁₅NO₆
Molecular Weight:305.287
Hs Code.:

Synonyms:5-[α-Carboxy-β-(4'-hydroxy-3',5'-dimethoxyphenyl) ethenyl]-3-methylisoxazole

Suppliers and Price of 5-[α-Carboxy-β-(4'-hydroxy-3',5'-dimethoxyphenyl) ethenyl]-3-methylisoxazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 5-[α-Carboxy-β-(4'-hydroxy-3',5'-dimethoxyphenyl) ethenyl]-3-methylisoxazole

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5-[α-Carboxy-β-(4'-hydroxy-3',5'-dimethoxyphenyl) ethenyl]-3-methylisoxazole

There total 2 articles about 5-[α-Carboxy-β-(4'-hydroxy-3',5'-dimethoxyphenyl) ethenyl]-3-methylisoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 5-[α-carbomethoxy-β-(4'-hydroxy-3',5'-dimethoxyphenyl)ethenyl]-3-methylisoxazole

: 113465-45-5
5-[α-Carboxy-β-(4'-hydroxy-3',5'-dimethoxyphenyl) ethenyl]-3-methylisoxazole

Guidance literature:: In aqueous KOH;

Reference yield:

: 134-96-3
syringic aldehyde

: 19668-85-0
2-(3-methylisoxazol-5-yl)acetic acid

: 113465-45-5
5-[α-Carboxy-β-(4'-hydroxy-3',5'-dimethoxyphenyl) ethenyl]-3-methylisoxazole

Guidance literature:: With piperidine; acetic acid; In toluene; for 3h; Heating;
DOI:10.1021/jm00106a006

Reference yield:

: 113465-45-5
5-[α-Carboxy-β-(4'-hydroxy-3',5'-dimethoxyphenyl) ethenyl]-3-methylisoxazole

: 113482-91-0
3-[β-(4'-hydroxy-3',5'-dimethoxyphenyl)ethenyl]-5-methylpyrazole

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 4 h / Heating

2: molybdenum hexacarbonyl, H₂O / acetonitrile / 12 h / Heating

3: 97percent hydrazine, acetic acid / 12 h / Ambient temperature

With pyridine; molybdenum hexacarbonyl; water; hydrazine hydrate; acetic acid; In acetonitrile;
DOI:10.1021/jm00106a006