C₅₀H₆₄N₂O₄Si₂

Base Information

Chemical Name:C₅₀H₆₄N₂O₄Si₂
CAS No.:141810-26-6
Molecular Formula:C₅₀H₆₄N₂O₄Si₂
Molecular Weight:813.24
Hs Code.:

C<sub>50</sub>H<sub>64</sub>N<sub>2</sub>O<sub>4</sub>Si<sub>2</sub>

Synonyms:C₅₀H₆₄N₂O₄Si₂

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Chemical Property of C₅₀H₆₄N₂O₄Si₂

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Technology Process of C₅₀H₆₄N₂O₄Si₂

There total 9 articles about C₅₀H₆₄N₂O₄Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 141810-25-5
C₃₄H₄₆N₂O₄Si

: 58479-61-1
tert-butylchlorodiphenylsilane

: 141810-26-6
C₅₀H₆₄N₂O₄Si₂

Guidance literature:: With dmap; triethylamine; In dichloromethane; for 22h; Ambient temperature;
DOI:10.1016/S0040-4020(01)88525-2

Reference yield:

: 2552-93-4
C₂₂H₃₂N₄O

: 141810-26-6
C₅₀H₆₄N₂O₄Si₂

Guidance literature:: Multi-step reaction with 7 steps

1: 1 N NaOH / CH₂Cl₂ / 0.5 h / Ambient temperature

2: 84 percent / CuCl₂ / tetrahydrofuran; H₂O / Ambient temperature; phosphate buffer pH 7

3: 71 percent / Et₃N / CH₂Cl₂ / 2.5 h / 0 °C

4: 78 percent / N-bromosuccinimide / tetrahydrofuran / 2 h / -22 °C

5: 71 percent / 1,8-diazabicyclo<5.4.0>undec-7-ene / dimethylformamide / 65 h / Ambient temperature

6: 98 percent / NaBH₄ / methanol / 0.67 h / Ambient temperature

7: 100 percent / Et₃N, p-dimethylaminopyridine / CH₂Cl₂ / 22 h / Ambient temperature

With dmap; sodium hydroxide; sodium tetrahydroborate; N-Bromosuccinimide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; copper dichloride; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)88525-2

Reference yield:

: 4360-12-7
(+)-ajmaline

: 141810-26-6
C₅₀H₆₄N₂O₄Si₂

Guidance literature:: Multi-step reaction with 8 steps

1: molecular sieves, H₂SO₄ / ethanol / 3 h / Heating

2: 1 N NaOH / CH₂Cl₂ / 0.5 h / Ambient temperature

3: 84 percent / CuCl₂ / tetrahydrofuran; H₂O / Ambient temperature; phosphate buffer pH 7

4: 71 percent / Et₃N / CH₂Cl₂ / 2.5 h / 0 °C

5: 78 percent / N-bromosuccinimide / tetrahydrofuran / 2 h / -22 °C

6: 71 percent / 1,8-diazabicyclo<5.4.0>undec-7-ene / dimethylformamide / 65 h / Ambient temperature

7: 98 percent / NaBH₄ / methanol / 0.67 h / Ambient temperature

8: 100 percent / Et₃N, p-dimethylaminopyridine / CH₂Cl₂ / 22 h / Ambient temperature

With dmap; sodium hydroxide; sodium tetrahydroborate; N-Bromosuccinimide; molecular sieve; sulfuric acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; copper dichloride; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)88525-2