(αR,α'R,4R,5R)-α,α'-diethyl-2,2-dimethyl-α,α'-diphenyl-1,3-dioxolane-4,5-dimethanol

Base Information

Chemical Name:(αR,α'R,4R,5R)-α,α'-diethyl-2,2-dimethyl-α,α'-diphenyl-1,3-dioxolane-4,5-dimethanol
CAS No.:911207-90-4
Molecular Formula:C₂₃H₃₀O₄
Molecular Weight:370.489
Hs Code.:

Synonyms:(αR,α'R,4R,5R)-α,α'-diethyl-2,2-dimethyl-α,α'-diphenyl-1,3-dioxolane-4,5-dimethanol

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Chemical Property of (αR,α'R,4R,5R)-α,α'-diethyl-2,2-dimethyl-α,α'-diphenyl-1,3-dioxolane-4,5-dimethanol

Chemical Property:

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Technology Process of (αR,α'R,4R,5R)-α,α'-diethyl-2,2-dimethyl-α,α'-diphenyl-1,3-dioxolane-4,5-dimethanol

There total 4 articles about (αR,α'R,4R,5R)-α,α'-diethyl-2,2-dimethyl-α,α'-diphenyl-1,3-dioxolane-4,5-dimethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: phenylmagnesium bromide

: 167282-09-9
(-)-((4R,5R)-5-benzoyl-2,2-dimethyl-[1,3]dioxolan-4-yl)-phenyl-methanone

: (αR,α'S,4R,5R)-α,α'-diethyl-2,2-dimethyl-α,α'-diphenyl-1,3-dioxolane-4,5-dimethanol

: 911207-90-4
(αR,α'R,4R,5R)-α,α'-diethyl-2,2-dimethyl-α,α'-diphenyl-1,3-dioxolane-4,5-dimethanol

Guidance literature:: In tetrahydrofuran; at -78 ℃;
DOI:10.1016/j.tetasy.2006.07.007

Reference yield:

: phenylmagnesium bromide

: 911207-90-4
(αR,α'R,4R,5R)-α,α'-diethyl-2,2-dimethyl-α,α'-diphenyl-1,3-dioxolane-4,5-dimethanol

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / -78 °C

In tetrahydrofuran; 1: Grignard reaction / 2: Grignard reaction;
DOI:10.1016/j.tetasy.2006.07.007

Reference yield:

: 177283-77-1
(4R,5R)-N,N'-dimethoxy-N,N',2,2-tetramethyl-1,3-dioxolane-4,5-dicarboxamide

: 911207-90-4
(αR,α'R,4R,5R)-α,α'-diethyl-2,2-dimethyl-α,α'-diphenyl-1,3-dioxolane-4,5-dimethanol

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / -78 °C

In tetrahydrofuran; 1: Grignard reaction / 2: Grignard reaction;
DOI:10.1016/j.tetasy.2006.07.007