3-(2-methyl-5-nitrophenyl)isoxazole-5-carbonyl chloride hydrochloride

Base Information

Chemical Name:3-(2-methyl-5-nitrophenyl)isoxazole-5-carbonyl chloride hydrochloride
CAS No.:943641-39-2
Molecular Formula:C₁₁H₇ClN₂O₄*ClH
Molecular Weight:303.102
Hs Code.:

Synonyms:3-(2-methyl-5-nitrophenyl)isoxazole-5-carbonyl chloride hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(2-methyl-5-nitrophenyl)isoxazole-5-carbonyl chloride hydrochloride

Chemical Property:

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Technology Process of 3-(2-methyl-5-nitrophenyl)isoxazole-5-carbonyl chloride hydrochloride

There total 1 articles about 3-(2-methyl-5-nitrophenyl)isoxazole-5-carbonyl chloride hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 943641-06-3
tert-butyl 3-(2-methyl-5-nitrophenyl)isoxazole-5-carboxylate

: 943641-39-2
3-(2-methyl-5-nitrophenyl)isoxazole-5-carbonyl chloride hydrochloride

Guidance literature:: tert-butyl 3-(2-methyl-5-nitrophenyl)isoxazole-5-carboxylate; With water; trifluoroacetic acid; In dichloromethane; for 1h;

With oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane; for 4h;

Reference yield:

: 943641-39-2
3-(2-methyl-5-nitrophenyl)isoxazole-5-carbonyl chloride hydrochloride

: 536-74-3
phenylacetylene

: 943641-41-6
1-(3-(2-methyl-5-nitrophenyl)isoxazol-5-yl)-3-phenylprop-2-yn-1-one

Guidance literature:: 3-(2-methyl-5-nitrophenyl)isoxazole-5-carbonyl chloride hydrochloride; phenylacetylene; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In tetrahydrofuran; for 0.166667h;

With triethylamine; In tetrahydrofuran; for 0.5h;