C₂₅H₄₂O₃S₂Si

Base Information

Chemical Name:C₂₅H₄₂O₃S₂Si
CAS No.:1598426-62-0
Molecular Formula:C₂₅H₄₂O₃S₂Si
Molecular Weight:482.824
Hs Code.:

C<sub>25</sub>H<sub>42</sub>O<sub>3</sub>S<sub>2</sub>Si

Synonyms:C₂₅H₄₂O₃S₂Si

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Chemical Property of C₂₅H₄₂O₃S₂Si

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Technology Process of C₂₅H₄₂O₃S₂Si

There total 5 articles about C₂₅H₄₂O₃S₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1197214-81-5
(Z)-4-(1,3-dithian-2-yl)but-2-en-1-ol

: 1598426-59-5
C₁₇H₂₉IO₂Si

: 1598426-62-0
C₂₅H₄₂O₃S₂Si

Guidance literature:: (Z)-4-(1,3-dithian-2-yl)but-2-en-1-ol; With N,N,N,N,N,N-hexamethylphosphoric triamide; tert.-butyl lithium; In tetrahydrofuran; pentane; at -78 ℃; for 0.0833333h; Inert atmosphere;

C₁₇H₂₉IO₂Si; In tetrahydrofuran; pentane; at -78 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ol500773w

Reference yield:

: 1598426-57-3
C₁₇H₃₀O₃Si

: 1598426-62-0
C₂₅H₄₂O₃S₂Si

Guidance literature:: Multi-step reaction with 2 steps

1.1: triphenylphosphine; 1H-imidazole; iodine / diethyl ether; acetonitrile / 0.5 h / 0 - 25 °C / Inert atmosphere

2.1: N,N,N,N,N,N-hexamethylphosphoric triamide; tert.-butyl lithium / tetrahydrofuran; pentane / 0.08 h / -78 °C / Inert atmosphere

2.2: 1 h / -78 °C / Inert atmosphere

With 1H-imidazole; N,N,N,N,N,N-hexamethylphosphoric triamide; iodine; tert.-butyl lithium; triphenylphosphine; In tetrahydrofuran; diethyl ether; acetonitrile; pentane;
DOI:10.1021/ol500773w

Reference yield:

: 69739-34-0
t-butyldimethylsiyl triflate

: 1598426-62-0
C₂₅H₄₂O₃S₂Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

2.1: ozone; triphenylphosphine / dichloromethane; methanol / 1 h / -78 - 25 °C / Inert atmosphere

2.2: 0.5 h / 25 °C / Inert atmosphere

3.1: triphenylphosphine; 1H-imidazole; iodine / diethyl ether; acetonitrile / 0.5 h / 0 - 25 °C / Inert atmosphere

4.1: N,N,N,N,N,N-hexamethylphosphoric triamide; tert.-butyl lithium / tetrahydrofuran; pentane / 0.08 h / -78 °C / Inert atmosphere

4.2: 1 h / -78 °C / Inert atmosphere

With 1H-imidazole; N,N,N,N,N,N-hexamethylphosphoric triamide; iodine; tert.-butyl lithium; ozone; triethylamine; triphenylphosphine; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; acetonitrile; pentane;
DOI:10.1021/ol500773w