1-benzyl-3-(4-acetoxybutyl)-4-((1'S)-1-phenylethyl)piperazine-2,5-dione

Base Information

Chemical Name:1-benzyl-3-(4-acetoxybutyl)-4-((1'S)-1-phenylethyl)piperazine-2,5-dione
CAS No.:1040726-61-1
Molecular Formula:C₂₅H₃₀N₂O₄
Molecular Weight:422.524
Hs Code.:

Synonyms:1-benzyl-3-(4-acetoxybutyl)-4-((1'S)-1-phenylethyl)piperazine-2,5-dione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-benzyl-3-(4-acetoxybutyl)-4-((1'S)-1-phenylethyl)piperazine-2,5-dione

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Technology Process of 1-benzyl-3-(4-acetoxybutyl)-4-((1'S)-1-phenylethyl)piperazine-2,5-dione

There total 2 articles about 1-benzyl-3-(4-acetoxybutyl)-4-((1'S)-1-phenylethyl)piperazine-2,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 1040726-57-5
5-benzylcarbamoyl-5-[(2-chloroacetyl)-((S)-1-phenylethyl)amino]pentyl acetate

: 1040726-61-1
1-benzyl-3-(4-acetoxybutyl)-4-((1'S)-1-phenylethyl)piperazine-2,5-dione

Guidance literature:: With caesium carbonate; In acetonitrile; at 20 ℃; for 2h;
DOI:10.1002/jhet.5570450321

Reference yield:

: 18545-16-9
5-acetoxypentanal

: 88333-03-3,10340-91-7
Benzyl isocyanide

: 2627-86-3
(S)-1-phenyl-ethylamine

: 79-11-8
chloroacetic acid

: 1040726-61-1
1-benzyl-3-(4-acetoxybutyl)-4-((1'S)-1-phenylethyl)piperazine-2,5-dione

Guidance literature:: 5-acetoxypentanal; Benzyl isocyanide; (S)-1-phenyl-ethylamine; chloroacetic acid; In methanol; at 20 ℃; for 120h;

With caesium carbonate; In acetonitrile; at 20 ℃; for 2h;
DOI:10.1016/j.tetasy.2017.08.004

Reference yield:

: 1040726-61-1
1-benzyl-3-(4-acetoxybutyl)-4-((1'S)-1-phenylethyl)piperazine-2,5-dione

: (1'S,3R)-1-benzyl-3-(4-hydroxybutyl)-4-(1-phenylethyl)piperazine-2,5-dione

: 1-benzyl-(3S)-3-(4-hydroxybutyl)-4-((1'S)-1-phenylethyl)piperazine-2,5-dione

: 1-benzyl-(3R)-3-(4-acetoxybutyl)-4-((1'S)-1-phenylethyl)-piperazine-2,5-dione

: C₂₅H₃₀N₂O₄

Guidance literature:: With immobilized Candida antarctica type B lipase; In aq. phosphate buffer; acetone; at 26 ℃; for 43h; pH=7.4; diastereoselective reaction; Enzymatic reaction;
DOI:10.1016/j.tetasy.2017.08.004