Dibenzyl-phosphinic acid 1,3-dioxo-1,3-dihydro-isoindol-2-ylmethyl ester

Base Information

Chemical Name:Dibenzyl-phosphinic acid 1,3-dioxo-1,3-dihydro-isoindol-2-ylmethyl ester
CAS No.:76219-47-1
Molecular Formula:C₂₃H₂₀NO₄P
Molecular Weight:405.39
Hs Code.:

Synonyms:Dibenzyl-phosphinic acid 1,3-dioxo-1,3-dihydro-isoindol-2-ylmethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Dibenzyl-phosphinic acid 1,3-dioxo-1,3-dihydro-isoindol-2-ylmethyl ester

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Technology Process of Dibenzyl-phosphinic acid 1,3-dioxo-1,3-dihydro-isoindol-2-ylmethyl ester

There total 2 articles about Dibenzyl-phosphinic acid 1,3-dioxo-1,3-dihydro-isoindol-2-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 5332-26-3
N-(bromomethyl)phtalimide

: 76219-39-1
Dibenzylphosphinic acid potassium salt

: 76219-47-1
Dibenzyl-phosphinic acid 1,3-dioxo-1,3-dihydro-isoindol-2-ylmethyl ester

Guidance literature:: With crown ether; In acetonitrile; for 3.5h; Heating;
DOI:10.1055/s-1980-29147

Reference yield:

: 7369-51-9
dibenzylphosphinic acid

: 76219-47-1
Dibenzyl-phosphinic acid 1,3-dioxo-1,3-dihydro-isoindol-2-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / potassium carbonate / H₂O

2: 91 percent / crown ether / acetonitrile / 3.5 h / Heating

With crown ether; potassium carbonate; In water; acetonitrile;
DOI:10.1055/s-1980-29147