carbonic acid 4-({[2-(bis-pyridin-2-ylmethyl-amino)-ethyl]-tert-butoxycarbonyl-amino}-methyl)-2-tert-butoxycarbonyloxy-phenyl ester tert-butyl ester

Base Information

Chemical Name:carbonic acid 4-({[2-(bis-pyridin-2-ylmethyl-amino)-ethyl]-tert-butoxycarbonyl-amino}-methyl)-2-tert-butoxycarbonyloxy-phenyl ester tert-butyl ester
CAS No.:851372-95-7
Molecular Formula:C₃₆H₄₈N₄O₈
Molecular Weight:664.799
Hs Code.:

carbonic acid 4-({[2-(bis-pyridin-2-ylmethyl-amino)-ethyl]-<i>tert</i>-butoxycarbonyl-amino}-methyl)-2-<i>tert</i>-butoxycarbonyloxy-phenyl ester <i>tert</i>-butyl ester

Synonyms:carbonic acid 4-({[2-(bis-pyridin-2-ylmethyl-amino)-ethyl]-tert-butoxycarbonyl-amino}-methyl)-2-tert-butoxycarbonyloxy-phenyl ester tert-butyl ester

Suppliers and Price of carbonic acid 4-({[2-(bis-pyridin-2-ylmethyl-amino)-ethyl]-tert-butoxycarbonyl-amino}-methyl)-2-tert-butoxycarbonyloxy-phenyl ester tert-butyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of carbonic acid 4-({[2-(bis-pyridin-2-ylmethyl-amino)-ethyl]-tert-butoxycarbonyl-amino}-methyl)-2-tert-butoxycarbonyloxy-phenyl ester tert-butyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of carbonic acid 4-({[2-(bis-pyridin-2-ylmethyl-amino)-ethyl]-tert-butoxycarbonyl-amino}-methyl)-2-tert-butoxycarbonyloxy-phenyl ester tert-butyl ester

There total 4 articles about carbonic acid 4-({[2-(bis-pyridin-2-ylmethyl-amino)-ethyl]-tert-butoxycarbonyl-amino}-methyl)-2-tert-butoxycarbonyloxy-phenyl ester tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 189440-33-3
(2-aminoethyl)bis(2-pyridylmethyl)amine

: 851372-95-7
carbonic acid 4-({[2-(bis-pyridin-2-ylmethyl-amino)-ethyl]-tert-butoxycarbonyl-amino}-methyl)-2-tert-butoxycarbonyloxy-phenyl ester tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: AcOH / propan-2-ol / 0.17 h / 50 °C

2: NaBH₄; AcOH / methanol / 0.5 h / 20 °C

3: 1.75 g / Et₃N / CH₂Cl₂ / 20 °C

With sodium tetrahydroborate; acetic acid; triethylamine; In methanol; dichloromethane; isopropyl alcohol;
DOI:10.1021/ja0455603

Reference yield:

: 851510-32-2
4-(2-(bis(2-pyridylmethyl)amino)ethylaminomethyl)1,2-benzenediol

: 24424-99-5
di-tert-butyl dicarbonate

: 851372-95-7
carbonic acid 4-({[2-(bis-pyridin-2-ylmethyl-amino)-ethyl]-tert-butoxycarbonyl-amino}-methyl)-2-tert-butoxycarbonyloxy-phenyl ester tert-butyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1021/ja0455603

Reference yield:

: 4-{[(Z)-2-(Bis-pyridin-2-ylmethyl-amino)-ethylimino]-methyl}-benzene-1,2-diol

: 851372-95-7
carbonic acid 4-({[2-(bis-pyridin-2-ylmethyl-amino)-ethyl]-tert-butoxycarbonyl-amino}-methyl)-2-tert-butoxycarbonyloxy-phenyl ester tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH₄; AcOH / methanol / 0.5 h / 20 °C

2: 1.75 g / Et₃N / CH₂Cl₂ / 20 °C

With sodium tetrahydroborate; acetic acid; triethylamine; In methanol; dichloromethane;
DOI:10.1021/ja0455603