1-(p-sulfamoylphenyl)-4-(N-methylene-1,6-dideoxy-1,6-imino-L-iditol)-1,2,3-triazole

Base Information

Chemical Name:1-(p-sulfamoylphenyl)-4-(N-methylene-1,6-dideoxy-1,6-imino-L-iditol)-1,2,3-triazole
CAS No.:1235555-06-2
Molecular Formula:C₁₅H₂₁N₅O₆S
Molecular Weight:399.428
Hs Code.:

Synonyms:1-(p-sulfamoylphenyl)-4-(N-methylene-1,6-dideoxy-1,6-imino-L-iditol)-1,2,3-triazole

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Chemical Property of 1-(p-sulfamoylphenyl)-4-(N-methylene-1,6-dideoxy-1,6-imino-L-iditol)-1,2,3-triazole

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Technology Process of 1-(p-sulfamoylphenyl)-4-(N-methylene-1,6-dideoxy-1,6-imino-L-iditol)-1,2,3-triazole

There total 3 articles about 1-(p-sulfamoylphenyl)-4-(N-methylene-1,6-dideoxy-1,6-imino-L-iditol)-1,2,3-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1235555-05-1
1-(p-sulfamoylphenyl)-4-(N-methylene-2,3,4,5-tetra-O-acetyl-1,6-dideoxy-1,6-imino-L-iditol)-1,2,3-triazole

: 1235555-06-2
1-(p-sulfamoylphenyl)-4-(N-methylene-1,6-dideoxy-1,6-imino-L-iditol)-1,2,3-triazole

Guidance literature:: With methanol; sodium methylate; at 20 ℃; for 0.5h;
DOI:10.1071/CH09426

Reference yield:

: 313054-61-4
3,4-di-O-(2-methoxybenzyl)-D-mannitol

: 1235555-06-2
1-(p-sulfamoylphenyl)-4-(N-methylene-1,6-dideoxy-1,6-imino-L-iditol)-1,2,3-triazole

Guidance literature:: Multi-step reaction with 8 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 0 °C / Inert atmosphere

2: triethylamine / dichloromethane / 0 °C / Inert atmosphere

3: hydrogenchloride; water / methanol / 0 °C

4: water; potassium hydroxide / methanol / 20 °C

5: methanol / 45 °C

6: water; trifluoroacetic acid / 20 °C

7: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 0.5 h / 40 °C

8: methanol; sodium methylate / 0.5 h / 20 °C

With 1H-imidazole; hydrogenchloride; methanol; copper(ll) sulfate pentahydrate; water; sodium methylate; sodium L-ascorbate; triethylamine; trifluoroacetic acid; potassium hydroxide; In methanol; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1071/CH09426

Reference yield:

: 1235554-97-8
2,3,4,5-tetra-O-acetyl-1,6-dideoxy-1,6-imino-N-propynyl-L-iditol

: 36326-86-0
4-azidobenzenesulfonamide

: 1235555-06-2
1-(p-sulfamoylphenyl)-4-(N-methylene-1,6-dideoxy-1,6-imino-L-iditol)-1,2,3-triazole

Guidance literature:: Multi-step reaction with 2 steps

1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 0.5 h / 40 °C

2: methanol; sodium methylate / 0.5 h / 20 °C

With methanol; copper(ll) sulfate pentahydrate; sodium methylate; sodium L-ascorbate; In water; tert-butyl alcohol;
DOI:10.1071/CH09426