Carbamic acid, [(1Z)-2-(acetylamino)ethenyl]-, 1,1-dimethylethyl ester (9CI)

Base Information

Chemical Name:Carbamic acid, [(1Z)-2-(acetylamino)ethenyl]-, 1,1-dimethylethyl ester (9CI)
CAS No.:240143-60-6
Molecular Formula:C₉H₁₆N₂O₃
Molecular Weight:200.238
Hs Code.:
Mol file:240143-60-6.mol

Synonyms:Carbamic acid, [(1Z)-2-(acetylamino)ethenyl]-, 1,1-dimethylethyl ester (9CI)

Suppliers and Price of Carbamic acid, [(1Z)-2-(acetylamino)ethenyl]-, 1,1-dimethylethyl ester (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of Carbamic acid, [(1Z)-2-(acetylamino)ethenyl]-, 1,1-dimethylethyl ester (9CI)

Chemical Property:

Boiling Point:329.6±38.0 °C(Predicted)
PKA:9.90±0.46(Predicted)
PSA：67.43000
Density:1.059±0.06 g/cm3(Predicted)
LogP:1.90020

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Carbamic acid, [(1Z)-2-(acetylamino)ethenyl]-, 1,1-dimethylethyl ester (9CI)

There total 2 articles about Carbamic acid, [(1Z)-2-(acetylamino)ethenyl]-, 1,1-dimethylethyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 240143-60-6
(2-acetylamino-vinyl)-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / ethyl acetate / 2 h / 0 - 20 °C

2: 1.) NaHCO₃, 2.) NaOH / 1.) ethyl acetate, 6 h, 2.) THF, 3 h

With sodium hydroxide; sodium hydrogencarbonate; triethylamine; In ethyl acetate;
DOI:10.1016/S0960-894X(99)00280-2

Reference yield:

: 108-24-7
acetic anhydride

: 49761-82-2
tert-butyl 1H-imidazole-1-carboxylate

: 240143-60-6
(2-acetylamino-vinyl)-carbamic acid tert-butyl ester

Guidance literature:: With sodium hydroxide; sodium hydrogencarbonate; Yield given; Multistep reaction; 1.) ethyl acetate, 6 h, 2.) THF, 3 h;
DOI:10.1016/S0960-894X(99)00280-2