C₃₆H₅₂N₂O₈S

Base Information

• Chemical Name: C₃₆H₅₂N₂O₈S
• CAS No.: 231307-22-5
• Molecular Formula: C₃₆H₅₂N₂O₈S
• Molecular Weight: 672.883
• Mol file: 231307-22-5.mol

Synonyms:C₃₆H₅₂N₂O₈S

Chemical Property of C₃₆H₅₂N₂O₈S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₆H₅₂N₂O₈S

There total 2 articles about C₃₆H₅₂N₂O₈S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

C36H52N2O6S (231307-19-0) → C36H52N2O8S (231307-22-5)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃;

DOI:10.1016/S0040-4039(99)00569-9

Reference yield:

[(1S,2S)-1-Benzyl-3-((2S,3S)-3-tert-butoxycarbonylamino-2-hydroxy-4-phenyl-butylsulfanyl)-2-hydroxy-propyl]-carbamic acid tert-butyl ester (228850-43-9) → C36H52N2O8S (231307-22-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 72 percent / p-toluenesulfonic acid / benzene / Heating

2: 100 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 20 °C

With toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; benzene; 1: Condensation / 2: Oxidation;

DOI:10.1016/S0040-4039(99)00569-9

Reference yield: 59.0%

C36H52N2O8S (231307-22-5) → C36H50N2O6

Guidance literature:

With aluminum oxide; potassium hydroxide; dibromodifluoromethane; In tert-butyl alcohol; at 20 ℃; for 4h;

DOI:10.1016/S0040-4039(99)00569-9

upstream raw materials:

C₃₆H₅₂N₂O₆S

[(1S,2S)-1-Benzyl-3-((2S,3S)-3-tert-butoxycarbonylamino-2-hydroxy-4-phenyl-butylsulfanyl)-2-hydroxy-propyl]-carbamic acid tert-butyl ester

Downstream raw materials:

C₃₆H₅₂N₂O₆