Benzoic acid 4-acetoxy-1-methyl-3-oxo-4-phenylsulfanyl-cyclohexylmethyl ester

Base Information

Chemical Name:Benzoic acid 4-acetoxy-1-methyl-3-oxo-4-phenylsulfanyl-cyclohexylmethyl ester
CAS No.:60603-29-4
Molecular Formula:C₂₃H₂₄O₅S
Molecular Weight:412.507
Hs Code.:

Synonyms:Benzoic acid 4-acetoxy-1-methyl-3-oxo-4-phenylsulfanyl-cyclohexylmethyl ester

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Chemical Property of Benzoic acid 4-acetoxy-1-methyl-3-oxo-4-phenylsulfanyl-cyclohexylmethyl ester

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Technology Process of Benzoic acid 4-acetoxy-1-methyl-3-oxo-4-phenylsulfanyl-cyclohexylmethyl ester

There total 9 articles about Benzoic acid 4-acetoxy-1-methyl-3-oxo-4-phenylsulfanyl-cyclohexylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 60603-28-3
Benzoic acid 1-methyl-3-oxo-4-phenylsulfanyl-cyclohexylmethyl ester

: 546-67-8
lead(IV) tetraacetate

: 60603-29-4
Benzoic acid 4-acetoxy-1-methyl-3-oxo-4-phenylsulfanyl-cyclohexylmethyl ester

Guidance literature:: In benzene; for 0.166667h; Heating;
DOI:10.1021/ja00530a041

Reference yield:

: 60603-16-9
2-methoxy-3-phenylthiobuta-1,3-diene

: 60603-29-4
Benzoic acid 4-acetoxy-1-methyl-3-oxo-4-phenylsulfanyl-cyclohexylmethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 2,6-di-tert-butyl-4-methylphenol / neat (no solvent) / Heating

2: 93 percent / sodium borohydride / methanol / 0.17 h / 0 °C

3: pyridine / 1 h / 0 °C

4: 228 mg / aq. perchloric acid / acetonitrile / 4 h / 0 °C

5: 89 percent / benzene / 0.17 h / Heating

With pyridine; sodium tetrahydroborate; perchloric acid; 2,6-di-tert-butyl-4-methyl-phenol; In methanol; acetonitrile; benzene;
DOI:10.1021/ja00530a041

Reference yield:

: 60603-23-8
3-methoxy-1-methyl-4-phenylthiocyclohex-3-ene-1-carboxaldehyde

: 60603-29-4
Benzoic acid 4-acetoxy-1-methyl-3-oxo-4-phenylsulfanyl-cyclohexylmethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / sodium borohydride / methanol / 0.17 h / 0 °C

2: pyridine / 1 h / 0 °C

3: 228 mg / aq. perchloric acid / acetonitrile / 4 h / 0 °C

4: 89 percent / benzene / 0.17 h / Heating

With pyridine; sodium tetrahydroborate; perchloric acid; In methanol; acetonitrile; benzene;
DOI:10.1021/ja00530a041