methyl 3-O-benzyl-4,6-O-benzylidene-2C-hydroxymethyl-β-D-glucopyranoside

Base Information

Chemical Name:methyl 3-O-benzyl-4,6-O-benzylidene-2C-hydroxymethyl-β-D-glucopyranoside
CAS No.:1313873-69-6
Molecular Formula:C₂₂H₂₆O₇
Molecular Weight:402.444
Hs Code.:

Synonyms:methyl 3-O-benzyl-4,6-O-benzylidene-2C-hydroxymethyl-β-D-glucopyranoside

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Chemical Property of methyl 3-O-benzyl-4,6-O-benzylidene-2C-hydroxymethyl-β-D-glucopyranoside

Chemical Property:

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Technology Process of methyl 3-O-benzyl-4,6-O-benzylidene-2C-hydroxymethyl-β-D-glucopyranoside

There total 3 articles about methyl 3-O-benzyl-4,6-O-benzylidene-2C-hydroxymethyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1313873-68-5
methyl 3-O-benzyl-4,6-O-benzylidene-2C-methylene-β-D-arabino-hexopyranoside

: 1313873-69-6
methyl 3-O-benzyl-4,6-O-benzylidene-2C-hydroxymethyl-β-D-glucopyranoside

Guidance literature:: With osmium(VIII) oxide; water; 4-methylmorpholine N-oxide; In acetone; tert-butyl alcohol; at 20 ℃; for 48h;
DOI:10.1002/chem.201003251

Reference yield:

: 129706-94-1
methyl 3-O-benzyl-4,6-O-benzylidene-β-D-arabino-hexopyranosid-2-ulose

: 1313873-69-6
methyl 3-O-benzyl-4,6-O-benzylidene-2C-hydroxymethyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran; hexanes / 2 h / 20 °C / Inert atmosphere

2: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / acetone; tert-butyl alcohol / 48 h / 20 °C

With osmium(VIII) oxide; water; 4-methylmorpholine N-oxide; In tetrahydrofuran; hexanes; acetone; tert-butyl alcohol;
DOI:10.1002/chem.201003251

Reference yield:

: 129706-93-0
methyl 3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside

: 1313873-69-6
methyl 3-O-benzyl-4,6-O-benzylidene-2C-hydroxymethyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1 h / -78 °C / Inert atmosphere

1.2: -78 - 20 °C / Inert atmosphere

2.1: tetrahydrofuran; hexanes / 2 h / 20 °C / Inert atmosphere

3.1: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / acetone; tert-butyl alcohol / 48 h / 20 °C

With osmium(VIII) oxide; oxalyl dichloride; water; dimethyl sulfoxide; 4-methylmorpholine N-oxide; In tetrahydrofuran; hexanes; dichloromethane; acetone; tert-butyl alcohol;
DOI:10.1002/chem.201003251