Technology Process of (2'R,3'S)-3'-p-tolyl-8,9-dihydrospiro[benzo[7]annulene-6,2'-oxiran]-5(7H)-one
There total 1 articles about (2'R,3'S)-3'-p-tolyl-8,9-dihydrospiro[benzo[7]annulene-6,2'-oxiran]-5(7H)-one which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
C28H34F6FeN6O6S2; dihydrogen peroxide; acetic acid;
In
dichloromethane; acetonitrile;
at -20 ℃;
for 2h;
optical yield given as %ee;
enantioselective reaction;
Inert atmosphere;
DOI:10.1002/chem.201200992