C₄₅H₆₂FN₅O₇

Base Information

Chemical Name:C₄₅H₆₂FN₅O₇
CAS No.:1009092-95-8
Molecular Formula:C₄₅H₆₂FN₅O₇
Molecular Weight:804.015
Hs Code.:

C<sub>45</sub>H<sub>62</sub>FN<sub>5</sub>O<sub>7</sub>

Synonyms:C₄₅H₆₂FN₅O₇

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Chemical Property of C₄₅H₆₂FN₅O₇

Chemical Property:

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Technology Process of C₄₅H₆₂FN₅O₇

There total 22 articles about C₄₅H₆₂FN₅O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.0%

: 1009092-94-7
C₁₁H₁₈N₂O

: 1009092-81-2
C₃₄H₄₆FN₃O₇

: 1009092-95-8
C₄₅H₆₂FN₅O₇

Guidance literature:: With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; In dichloromethane; for 14h;

Reference yield:

: 3-bromo-6-fluoro-2-hydroxybenzaldehyde

: 1009092-95-8
C₄₅H₆₂FN₅O₇

Guidance literature:: Multi-step reaction with 9 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 5 h / 40 °C

2.1: hydroxylamine hydrochloride / tetrahydrofuran; methanol; water / 0.08 h / 20 °C

3.1: hydrogenchloride; methyl orange; sodium cyanoborohydride / tetrahydrofuran; methanol; water / 3 h / pH 2

4.1: toluene / Heating / reflux

5.1: hydrogenchloride / tetrahydrofuran; water / 2 h / 20 °C

6.1: trimethylaluminum / hexanes; dichloromethane / 0.25 h

6.2: 20 °C

7.1: potassium acetate; caesium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide

8.1: sodium cyanoborohydride; acetic acid / methanol; water / 0.67 h / 20 °C

9.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / dichloromethane / 14 h

With hydrogenchloride; hydroxylamine hydrochloride; methyl orange; trimethylaluminum; potassium acetate; sodium cyanoborohydride; potassium carbonate; caesium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; acetic acid; triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; methanol; hexanes; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;

Reference yield:

: 473416-74-9
3-bromo-6-fluoro-2-methoxybenzaldehyde

: 1009092-95-8
C₄₅H₆₂FN₅O₇

Guidance literature:: Multi-step reaction with 8 steps

1.1: hydroxylamine hydrochloride / tetrahydrofuran; methanol; water / 0.08 h / 20 °C

2.1: hydrogenchloride; methyl orange; sodium cyanoborohydride / tetrahydrofuran; methanol; water / 3 h / pH 2

3.1: toluene / Heating / reflux

4.1: hydrogenchloride / tetrahydrofuran; water / 2 h / 20 °C

5.1: trimethylaluminum / hexanes; dichloromethane / 0.25 h

5.2: 20 °C

6.1: potassium acetate; caesium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / dimethyl sulfoxide

7.1: sodium cyanoborohydride; acetic acid / methanol; water / 0.67 h / 20 °C

8.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine / dichloromethane / 14 h

With hydrogenchloride; hydroxylamine hydrochloride; methyl orange; trimethylaluminum; potassium acetate; sodium cyanoborohydride; caesium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; acetic acid; triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; methanol; hexanes; dichloromethane; water; dimethyl sulfoxide; toluene;