C₂₉H₁₉BrO₈

Base Information

Chemical Name:C₂₉H₁₉BrO₈
CAS No.:1616873-22-3
Molecular Formula:C₂₉H₁₉BrO₈
Molecular Weight:575.369
Hs Code.:

C<sub>29</sub>H<sub>19</sub>BrO<sub>8</sub>

Synonyms:C₂₉H₁₉BrO₈

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Chemical Property of C₂₉H₁₉BrO₈

Chemical Property:

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Technology Process of C₂₉H₁₉BrO₈

There total 18 articles about C₂₉H₁₉BrO₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1616872-99-1
C₂₅H₃₁ClO₉

: 1616873-22-3
C₂₉H₁₉BrO₈

Guidance literature:: Multi-step reaction with 10 steps

1.1: sodium acetate; acetic acid / 12 h / 80 °C / Inert atmosphere

2.1: hydrogenchloride; water / methanol; tetrahydrofuran / 16 h / 50 °C

3.1: toluene-4-sulfonic acid / acetone / 0.33 h / Inert atmosphere

3.2: 0.33 h

4.1: triethylamine; dmap / dichloromethane / 2 h / 0 °C / Inert atmosphere

5.1: hydrogenchloride; water / methanol; tetrahydrofuran / 16 h / 50 °C

6.1: methanesulfonyl chloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 °C / Inert atmosphere

6.2: 1 h / 0 °C / Inert atmosphere

7.1: ammonium cerium (IV) nitrate / water; ethyl acetate; acetonitrile / 1.25 h / 0 °C

8.1: toluene / 12 h / 100 °C / Schlenk technique; Inert atmosphere

9.1: Jones reagent; potassium fluoride / acetone / 45 h / 0 °C / Inert atmosphere

10.1: triethylamine / 0.17 h / Inert atmosphere

With hydrogenchloride; dmap; potassium fluoride; Jones reagent; ammonium cerium (IV) nitrate; water; sodium acetate; toluene-4-sulfonic acid; acetic acid; methanesulfonyl chloride; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; acetone; toluene; acetonitrile; 8.1: |Diels-Alder Cycloaddition;
DOI:10.1002/chem.201402254

Reference yield:

: C₂₅H₃₃ClO₉

: 1616873-22-3
C₂₉H₁₉BrO₈

Guidance literature:: Multi-step reaction with 11 steps

1.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 20 h / 65 °C / Inert atmosphere

2.1: sodium acetate; acetic acid / 12 h / 80 °C / Inert atmosphere

3.1: hydrogenchloride; water / methanol; tetrahydrofuran / 16 h / 50 °C

4.1: toluene-4-sulfonic acid / acetone / 0.33 h / Inert atmosphere

4.2: 0.33 h

5.1: triethylamine; dmap / dichloromethane / 2 h / 0 °C / Inert atmosphere

6.1: hydrogenchloride; water / methanol; tetrahydrofuran / 16 h / 50 °C

7.1: methanesulfonyl chloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 °C / Inert atmosphere

7.2: 1 h / 0 °C / Inert atmosphere

8.1: ammonium cerium (IV) nitrate / water; ethyl acetate; acetonitrile / 1.25 h / 0 °C

9.1: toluene / 12 h / 100 °C / Schlenk technique; Inert atmosphere

10.1: Jones reagent; potassium fluoride / acetone / 45 h / 0 °C / Inert atmosphere

11.1: triethylamine / 0.17 h / Inert atmosphere

With hydrogenchloride; dmap; potassium fluoride; Jones reagent; ammonium cerium (IV) nitrate; water; sodium acetate; toluene-4-sulfonic acid; acetic acid; methanesulfonyl chloride; triethylamine; N-ethyl-N,N-diisopropylamine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; acetone; toluene; acetonitrile; 9.1: |Diels-Alder Cycloaddition;
DOI:10.1002/chem.201402254

Reference yield:

: 1616873-07-4
C₃₀H₂₉ClO₈

: 1616873-22-3
C₂₉H₁₉BrO₈

Guidance literature:: Multi-step reaction with 6 steps

1.1: hydrogenchloride; water / methanol; tetrahydrofuran / 16 h / 50 °C

2.1: methanesulfonyl chloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 °C / Inert atmosphere

2.2: 1 h / 0 °C / Inert atmosphere

3.1: ammonium cerium (IV) nitrate / water; ethyl acetate; acetonitrile / 1.25 h / 0 °C

4.1: toluene / 12 h / 100 °C / Schlenk technique; Inert atmosphere

5.1: Jones reagent; potassium fluoride / acetone / 45 h / 0 °C / Inert atmosphere

6.1: triethylamine / 0.17 h / Inert atmosphere

With hydrogenchloride; potassium fluoride; Jones reagent; ammonium cerium (IV) nitrate; water; methanesulfonyl chloride; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; water; ethyl acetate; acetone; toluene; acetonitrile; 4.1: |Diels-Alder Cycloaddition;
DOI:10.1002/chem.201402254