2,6-dichloro-4-(3-(piperazin-1-yl)phenyl)quinazoline trifluoroacetate

Base Information

• Chemical Name: 2,6-dichloro-4-(3-(piperazin-1-yl)phenyl)quinazoline trifluoroacetate
• CAS No.: 1234367-55-5
• Molecular Formula: C₂HF₃O₂*C₁₈H₁₆Cl₂N₄
• Molecular Weight: 473.282

Synonyms:2,6-dichloro-4-(3-(piperazin-1-yl)phenyl)quinazoline trifluoroacetate

Chemical Property of 2,6-dichloro-4-(3-(piperazin-1-yl)phenyl)quinazoline trifluoroacetate

Chemical Property:

Purity/Quality:

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Technology Process of 2,6-dichloro-4-(3-(piperazin-1-yl)phenyl)quinazoline trifluoroacetate

There total 1 articles about 2,6-dichloro-4-(3-(piperazin-1-yl)phenyl)quinazoline trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butyl 4-(3-(2,6-dichloroquinazolin-4-yl)phenyl)piperazine-1-carboxylate (1234367-53-3) + trifluoroacetic acid (76-05-1) → 2,6-dichloro-4-(3-(piperazin-1-yl)phenyl)quinazoline trifluoroacetate (1234367-55-5)

Guidance literature:

In dichloromethane; at 40 ℃; for 3h;

Reference yield: 77.0%

2,6-dichloro-4-(3-(piperazin-1-yl)phenyl)quinazoline trifluoroacetate (1234367-55-5) + 1,3-di(tert-butyloxycarbonyl)-2-(trifluoromethylsulfonyl)guanidine (207857-15-6) → tert-butyl (4-(3-(2,6-dichloroquinazolin-4-yl)phenyl)piperazin-1-yl)methanediylidenedicarbamate (1234367-56-6)

Guidance literature:

With triethylamine; In dichloromethane; at 40 ℃; for 3h;

Reference yield: 62.0%

2,3,4,5,6-penta-O-acetyl-D-gluconoyl chloride (53555-69-4) + 2,6-dichloro-4-(3-(piperazin-1-yl)phenyl)quinazoline trifluoroacetate (1234367-55-5) → C34H36Cl2N4O11 (1234367-61-3)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃;

upstream raw materials:

tert-butyl 4-(3-(2,6-dichloroquinazolin-4-yl)phenyl)piperazine-1-carboxylate

trifluoroacetic acid

Downstream raw materials:

methyl 3-(4-(3-(2,6-dichloroquinazolin-4-yl)phenyl)piperazin-1-yl)propanoate

tert-butyl (4-(3-(2,6-dichloroquinazolin-4-yl)phenyl)piperazin-1-yl)methanediylidenedicarbamate

C₃₄H₃₆Cl₂N₄O₁₁

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