1,6-Anhydro-2,3-di-O-benzyl-5-O-(trifluormethylsulfonyl)-α-L-idofuranose

Base Information

Chemical Name:1,6-Anhydro-2,3-di-O-benzyl-5-O-(trifluormethylsulfonyl)-α-L-idofuranose
CAS No.:118475-51-7
Molecular Formula:C₂₁H₂₁F₃O₇S
Molecular Weight:474.455
Hs Code.:

Synonyms:1,6-Anhydro-2,3-di-O-benzyl-5-O-(trifluormethylsulfonyl)-α-L-idofuranose

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Chemical Property of 1,6-Anhydro-2,3-di-O-benzyl-5-O-(trifluormethylsulfonyl)-α-L-idofuranose

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Technology Process of 1,6-Anhydro-2,3-di-O-benzyl-5-O-(trifluormethylsulfonyl)-α-L-idofuranose

There total 4 articles about 1,6-Anhydro-2,3-di-O-benzyl-5-O-(trifluormethylsulfonyl)-α-L-idofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 81937-01-1
1,6-Anhydro-2,3-di-O-benzyl-α-L-idofuranose

: 118475-51-7
1,6-Anhydro-2,3-di-O-benzyl-5-O-(trifluormethylsulfonyl)-α-L-idofuranose

Guidance literature:: With pyridine; In dichloromethane; at -10 ℃; for 0.333333h;

Reference yield:

: 81936-96-1
1,6-Anhydro-2,3-di-O-benzyl-β-D-xylo-hexofuranos-5-ulose

: 118475-51-7
1,6-Anhydro-2,3-di-O-benzyl-5-O-(trifluormethylsulfonyl)-α-L-idofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / aq. NaBH₄ / ethanol; dioxane / 1.5 h / Ambient temperature

2: 91 percent / pyridine / CH₂Cl₂ / 0.33 h / -10 °C

With pyridine; sodium tetrahydroborate; In 1,4-dioxane; ethanol; dichloromethane;

Reference yield:

: 51516-26-8
1,6-Anhydro-2,3-di-O-benzyl-β-D-glucofuranose

: 118475-51-7
1,6-Anhydro-2,3-di-O-benzyl-5-O-(trifluormethylsulfonyl)-α-L-idofuranose

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / pyridinium chlorochromate, NaOAc / CH₂Cl₂ / 6 h / Heating

2: 96 percent / aq. NaBH₄ / ethanol; dioxane / 1.5 h / Ambient temperature

3: 91 percent / pyridine / CH₂Cl₂ / 0.33 h / -10 °C

With pyridine; sodium tetrahydroborate; sodium acetate; pyridinium chlorochromate; In 1,4-dioxane; ethanol; dichloromethane;