N-(5-dioctylcarbamoyl-2-fluoro-4-methyl-phenyl)-2-fluoro-isophthalamic acid

Base Information

Chemical Name:N-(5-dioctylcarbamoyl-2-fluoro-4-methyl-phenyl)-2-fluoro-isophthalamic acid
CAS No.:925915-70-4
Molecular Formula:C₃₂H₄₄F₂N₂O₄
Molecular Weight:558.709
Hs Code.:

<i>N</i>-(5-dioctylcarbamoyl-2-fluoro-4-methyl-phenyl)-2-fluoro-isophthalamic acid

Synonyms:N-(5-dioctylcarbamoyl-2-fluoro-4-methyl-phenyl)-2-fluoro-isophthalamic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(5-dioctylcarbamoyl-2-fluoro-4-methyl-phenyl)-2-fluoro-isophthalamic acid

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Technology Process of N-(5-dioctylcarbamoyl-2-fluoro-4-methyl-phenyl)-2-fluoro-isophthalamic acid

There total 6 articles about N-(5-dioctylcarbamoyl-2-fluoro-4-methyl-phenyl)-2-fluoro-isophthalamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 925915-60-2
N-(5-dioctylcarbamoyl-2-fluoro-4-methyl-phenyl)-2-fluoro-isophthalamic acid methyl ester

: 925915-70-4
N-(5-dioctylcarbamoyl-2-fluoro-4-methyl-phenyl)-2-fluoro-isophthalamic acid

Guidance literature:: With lithium hydroxide; water; In tetrahydrofuran; at 20 ℃; for 5h;
DOI:10.1002/anie.200500982

Reference yield:

: 4-fluoro-2-methyl-5-nitrobenzoyl chloride

: 925915-70-4
N-(5-dioctylcarbamoyl-2-fluoro-4-methyl-phenyl)-2-fluoro-isophthalamic acid

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / Et₃N / CH₂Cl₂

2: 95 percent / H₂ / Pd/C / methanol; tetrahydrofuran / 24 h / 20 °C / 760 Torr

3: 91 percent / Et₃N / CH₂Cl₂ / 0.5 h / 20 °C

4: 98 percent / LiOH; H₂O / tetrahydrofuran / 5 h / 20 °C

With lithium hydroxide; water; hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1002/anie.200500982

Reference yield:

: 925915-38-4
4-fluoro-2-methyl-5-nitro-N,N-dioctyl-benzamide

: 925915-70-4
N-(5-dioctylcarbamoyl-2-fluoro-4-methyl-phenyl)-2-fluoro-isophthalamic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / H₂ / Pd/C / methanol; tetrahydrofuran / 24 h / 20 °C / 760 Torr

2: 91 percent / Et₃N / CH₂Cl₂ / 0.5 h / 20 °C

3: 98 percent / LiOH; H₂O / tetrahydrofuran / 5 h / 20 °C

With lithium hydroxide; water; hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1002/anie.200500982