TERT-BUTYL HEXAHYDRO-1H-PYRROLO[3,4-C]PYRIDINE-2(3H)-CARBOXYLATE

Base Information

• Chemical Name: TERT-BUTYL HEXAHYDRO-1H-PYRROLO[3,4-C]PYRIDINE-2(3H)-CARBOXYLATE
• CAS No.: 236406-56-7
• Molecular Formula: C₁₂H₂₂N₂O₂
• Molecular Weight: 226.319
• Hs Code.: 2933990090
• Mol file: 236406-56-7.mol

Synonyms:TERT-BUTYL HEXAHYDRO-1H-PYRROLO[3,4-C]PYRIDINE-2(3H)-CARBOXYLATE

Chemical Property of TERT-BUTYL HEXAHYDRO-1H-PYRROLO[3,4-C]PYRIDINE-2(3H)-CARBOXYLATE

Chemical Property:

• Vapor Pressure: 0.000485mmHg at 25°C
• Refractive Index: 1.489
• Boiling Point: 313.8°C at 760 mmHg
• PKA: 11.23±0.20(Predicted)
• Flash Point: 143.6°C
• PSA: 41.57000
• Density: 1.052g/cm³
• LogP: 1.72950

Purity/Quality:

97% ^*data from raw suppliers

Racemiccis-octahydro-pyrrolo[3,4-c]pyridine-2-carboxylicacidtert-butylester 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of TERT-BUTYL HEXAHYDRO-1H-PYRROLO[3,4-C]PYRIDINE-2(3H)-CARBOXYLATE

There total 3 articles about TERT-BUTYL HEXAHYDRO-1H-PYRROLO[3,4-C]PYRIDINE-2(3H)-CARBOXYLATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butyl 6-oxohexahydro-1H-pyrrolo[3,4-c]pyridine-2(3H)carboxylate → hexahydro-1H-pyrrolo[3,4-c]pyridine-2(3H)-carboxylic acid tert-butyl ester (885270-57-5,236406-56-7)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at -10 - 20 ℃; for 3h;

Reference yield:

tert-butyl 5-oxohexahydrocyclopenta[c]pyrrole-2(1H)-carboxylate (148404-28-8) → hexahydro-1H-pyrrolo[3,4-c]pyridine-2(3H)-carboxylic acid tert-butyl ester (885270-57-5,236406-56-7)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium azide; methanesulfonic acid / chloroform / 2 h / 70 °C

2: sodium hydride / tetrahydrofuran; water / 3 h / 20 °C

3: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / -10 - 20 °C

With lithium aluminium tetrahydride; sodium azide; methanesulfonic acid; sodium hydride; In tetrahydrofuran; chloroform; water;

Reference yield:

hexahydro-1H-pyrrolo[3,4-c]pyridin-6(2H)one → hexahydro-1H-pyrrolo[3,4-c]pyridine-2(3H)-carboxylic acid tert-butyl ester (885270-57-5,236406-56-7)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydride / tetrahydrofuran; water / 3 h / 20 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / -10 - 20 °C

With lithium aluminium tetrahydride; sodium hydride; In tetrahydrofuran; water;

upstream raw materials:

tert-butyl 5-oxohexahydrocyclopenta[c]pyrrole-2(1H)-carboxylate

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