4-(4'-hydroxyphenyl)-2-(4-chlorophenyl)-2,3-dihydro-1,5-benzothiazepine

Base Information

Chemical Name:4-(4'-hydroxyphenyl)-2-(4-chlorophenyl)-2,3-dihydro-1,5-benzothiazepine
CAS No.:308087-80-1
Molecular Formula:C₂₁H₁₆ClNOS
Molecular Weight:365.883
Hs Code.:

Synonyms:4-(4'-hydroxyphenyl)-2-(4-chlorophenyl)-2,3-dihydro-1,5-benzothiazepine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(4'-hydroxyphenyl)-2-(4-chlorophenyl)-2,3-dihydro-1,5-benzothiazepine

Chemical Property:

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Technology Process of 4-(4'-hydroxyphenyl)-2-(4-chlorophenyl)-2,3-dihydro-1,5-benzothiazepine

There total 4 articles about 4-(4'-hydroxyphenyl)-2-(4-chlorophenyl)-2,3-dihydro-1,5-benzothiazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 19152-38-6
1-(4-chlorophenyl)-3-(4-hydroxyphenyl)prop-2-enone

: 137-07-5
2-amino-benzenethiol

: 308087-80-1
4-(4'-hydroxyphenyl)-2-(4-chlorophenyl)-2,3-dihydro-1,5-benzothiazepine

Guidance literature:: With hydrogenchloride; sodium sulfate; In ethanol; water; Reflux;
DOI:10.1016/j.ejmech.2016.09.069

Reference yield:

: 104-88-1
4-chlorobenzaldehyde

: 308087-80-1
4-(4'-hydroxyphenyl)-2-(4-chlorophenyl)-2,3-dihydro-1,5-benzothiazepine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / ethanol

2: hydrogenchloride; sodium sulfate / ethanol; water / Reflux

With hydrogenchloride; sodium sulfate; sodium hydroxide; In ethanol; water;
DOI:10.1016/j.ejmech.2016.09.069

Reference yield:

: 99-93-4
4-Hydroxyacetophenone

: 308087-80-1
4-(4'-hydroxyphenyl)-2-(4-chlorophenyl)-2,3-dihydro-1,5-benzothiazepine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / ethanol

2: hydrogenchloride; sodium sulfate / ethanol; water / Reflux

With hydrogenchloride; sodium sulfate; sodium hydroxide; In ethanol; water;
DOI:10.1016/j.ejmech.2016.09.069