Technology Process of C25H32O6S2
There total 13 articles about C25H32O6S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 50 ℃;
for 9h;
Yield given;
DOI:10.1021/ja00344a047
- Guidance literature:
-
Multi-step reaction with 6 steps
1: tetrahydrofuran / 3 h / 40 °C
2: NaI / dimethylformamide / 3 h / 100 °C
3: K2CO3 / acetonitrile / 24 h / Heating
4: 90 percent / 1.) dimsyl sodium / 2.) DMSO, 25 deg C, 4 h
5: 75 percent / pyridine / CH2Cl2 / 4 h / 23 °C
6: tetra-n-butylammonium fluoride / tetrahydrofuran / 9 h / 50 °C
With
pyridine; tetrabutyl ammonium fluoride; sodium methylsulfinylmethanide; potassium carbonate; sodium iodide;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ja00344a047
- Guidance literature:
-
Multi-step reaction with 9 steps
1: 1.) trimethylchlorosilane, NaI / 1.) MeCN, 50 deg C, 4 h
2: 4-(dimethylamino)pyridine / CH2Cl2 / 0.5 h / 0 °C
3: K2CO3 / methanol / 1.5 h / 23 °C
4: 90 percent / diisopropylcarbodiimide, dichloroacetic acid / benzene; dimethylsulfoxide / 0.5 h / 23 °C
5: zinc triflate / CH2Cl2 / 5 h / 23 °C
6: diisobutylaluminum hydride / toluene / 0.5 h / -78 °C
7: 90 percent / 1.) dimsyl sodium / 2.) DMSO, 25 deg C, 4 h
8: 75 percent / pyridine / CH2Cl2 / 4 h / 23 °C
9: tetra-n-butylammonium fluoride / tetrahydrofuran / 9 h / 50 °C
With
pyridine; dichloro-acetic acid; dmap; chloro-trimethyl-silane; tetrabutyl ammonium fluoride; zinc trifluoromethanesulfonate; diisobutylaluminium hydride; sodium methylsulfinylmethanide; potassium carbonate; sodium iodide; diisopropyl-carbodiimide;
In
tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide; toluene; benzene;
DOI:10.1021/ja00344a047
