2,3,5-tri-O-benzyl-4-O-p-nitrobenzoyl-L-lyxose dithiobenzylacetal

Base Information

Chemical Name:2,3,5-tri-O-benzyl-4-O-p-nitrobenzoyl-L-lyxose dithiobenzylacetal
CAS No.:161424-49-3
Molecular Formula:C₄₇H₄₅NO₇S₂
Molecular Weight:800.009
Hs Code.:

Synonyms:2,3,5-tri-O-benzyl-4-O-p-nitrobenzoyl-L-lyxose dithiobenzylacetal

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Chemical Property of 2,3,5-tri-O-benzyl-4-O-p-nitrobenzoyl-L-lyxose dithiobenzylacetal

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Technology Process of 2,3,5-tri-O-benzyl-4-O-p-nitrobenzoyl-L-lyxose dithiobenzylacetal

There total 3 articles about 2,3,5-tri-O-benzyl-4-O-p-nitrobenzoyl-L-lyxose dithiobenzylacetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 153439-75-9
2,3,5-tri-O-benzyl-D-ribose dibenzyldithioacetal

: 62-23-7
4-nitro-benzoic acid

: 161424-49-3
2,3,5-tri-O-benzyl-4-O-p-nitrobenzoyl-L-lyxose dithiobenzylacetal

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; for 3h; Ambient temperature;
DOI:10.1080/15257779408013205

Reference yield:

: 64363-77-5
methyl 2,3,5-tri-O-benzyl-D-ribofuranoside

: 161424-49-3
2,3,5-tri-O-benzyl-4-O-p-nitrobenzoyl-L-lyxose dithiobenzylacetal

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / BF₃*Et₂O / 48 h / 0 °C

2: 80 percent / Ph₃P, DEAD / tetrahydrofuran / 3 h / Ambient temperature

With boron trifluoride diethyl etherate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran;
DOI:10.1080/15257779408013205

Reference yield:

: 100-53-8
phenylmethanethiol

: 161424-49-3
2,3,5-tri-O-benzyl-4-O-p-nitrobenzoyl-L-lyxose dithiobenzylacetal

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / BF₃*Et₂O / 48 h / 0 °C

2: 80 percent / Ph₃P, DEAD / tetrahydrofuran / 3 h / Ambient temperature

With boron trifluoride diethyl etherate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran;
DOI:10.1080/15257779408013205