(E)-1-(1,3-diphenylprop-1-en-1-yl)-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole

Base Information

Chemical Name:(E)-1-(1,3-diphenylprop-1-en-1-yl)-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole
CAS No.:1616670-81-5
Molecular Formula:C₂₆H₂₄N₂
Molecular Weight:364.49
Hs Code.:

Synonyms:(E)-1-(1,3-diphenylprop-1-en-1-yl)-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole

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Chemical Property of (E)-1-(1,3-diphenylprop-1-en-1-yl)-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole

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Technology Process of (E)-1-(1,3-diphenylprop-1-en-1-yl)-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole

There total 3 articles about (E)-1-(1,3-diphenylprop-1-en-1-yl)-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 61-54-1
tryptamine

: 343-94-2
tryptamine hydochloride

: 115872-75-8
(E)-2,4-diphenyl-but-2-enal

: 1616670-81-5
(E)-1-(1,3-diphenylprop-1-en-1-yl)-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole

Guidance literature:: tryptamine; tryptamine hydochloride; (E)-2,4-diphenyl-but-2-enal; In toluene; at 130 ℃; for 3h; Inert atmosphere;

With trifluoroacetic acid; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2014.05.068

Reference yield: 14.0%

: 61-54-1
tryptamine

: 343-94-2
tryptamine hydochloride

: 122-78-1
phenylacetaldehyde

: 3851-30-7,99545-51-4,122088-15-7
1-benzyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole

: 1616670-81-5
(E)-1-(1,3-diphenylprop-1-en-1-yl)-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole

Guidance literature:: tryptamine; tryptamine hydochloride; phenylacetaldehyde; In toluene; for 3h; Reflux; Inert atmosphere;

With trifluoroacetic acid; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2014.05.068

Reference yield:

: 122-78-1
phenylacetaldehyde

: 1616670-81-5
(E)-1-(1,3-diphenylprop-1-en-1-yl)-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole

Guidance literature:: Multi-step reaction with 2 steps

1.1: ammonium acetate / water; acetic acid; ethyl acetate / Inert atmosphere

2.1: toluene / 3 h / 130 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere

With ammonium acetate; In water; acetic acid; ethyl acetate; toluene; 2.1: |Pictet-Spengler Synthesis / 2.2: |Pictet-Spengler Synthesis;
DOI:10.1016/j.tet.2014.05.068