C₄₁H₆₄Si₂O₆

Base Information

Chemical Name:C₄₁H₆₄Si₂O₆
CAS No.:930807-77-5
Molecular Formula:C₄₁H₆₄O₆Si₂
Molecular Weight:709.127
Hs Code.:

C<sub>41</sub>H<sub>64</sub>Si<sub>2</sub>O<sub>6</sub>

Synonyms:C₄₁H₆₄Si₂O₆

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Chemical Property of C₄₁H₆₄Si₂O₆

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Technology Process of C₄₁H₆₄Si₂O₆

There total 4 articles about C₄₁H₆₄Si₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 930807-76-4
C₄₀H₆₂Si₂O₇

: dimethyl titanocene

: 930807-77-5
C₄₁H₆₄Si₂O₆

Guidance literature:: With 2,2-dimethyl-propanoic acid ethyl ester; In tetrahydrofuran; toluene; at 80 ℃; for 15h;
DOI:10.1002/anie.200603656

Reference yield:

: 930807-74-2
C₃₄H₅₀O₇Si

: 930807-77-5
C₄₁H₆₄Si₂O₆

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / 2,6-lutidine / CH₂Cl₂ / 1.25 h / -78 °C

2: 94 percent / Dess-Martin periodinane / CH₂Cl₂ / 2 h / 20 °C

3: 77 percent / ethyl pivalate / tetrahydrofuran; toluene / 15 h / 80 °C

With 2,6-dimethylpyridine; 2,2-dimethyl-propanoic acid ethyl ester; Dess-Martin periodane; In tetrahydrofuran; dichloromethane; toluene; 2: Dess-Martin oxidation;
DOI:10.1002/anie.200603656

Reference yield:

: 930807-75-3
C₄₀H₆₄Si₂O₇

: 930807-77-5
C₄₁H₆₄Si₂O₆

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / Dess-Martin periodinane / CH₂Cl₂ / 2 h / 20 °C

2: 77 percent / ethyl pivalate / tetrahydrofuran; toluene / 15 h / 80 °C

With 2,2-dimethyl-propanoic acid ethyl ester; Dess-Martin periodane; In tetrahydrofuran; dichloromethane; toluene; 1: Dess-Martin oxidation;
DOI:10.1002/anie.200603656