Technology Process of C37H37N7O12S
There total 5 articles about C37H37N7O12S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
copper(ll) sulfate pentahydrate; sodium L-ascorbate;
In
water; dimethyl sulfoxide;
at 20 ℃;
DOI:10.1039/c2ob25428j
- Guidance literature:
-
Multi-step reaction with 4 steps
1: benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide / water; N,N-dimethyl-formamide / 75 °C
2: trifluoroacetic acid / dichloromethane / 3 h / 0 - 20 °C
3: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 5 h / 20 °C
4: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; dimethyl sulfoxide / 20 °C
With
copper(ll) sulfate pentahydrate; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; benzotriazol-1-ol; sodium L-ascorbate; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid;
In
dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
4: Huisgen 1,3-dipolar cycloaddition;
DOI:10.1039/c2ob25428j
- Guidance literature:
-
Multi-step reaction with 4 steps
1: benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide / water; N,N-dimethyl-formamide / 75 °C
2: trifluoroacetic acid / dichloromethane / 3 h / 0 - 20 °C
3: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 5 h / 20 °C
4: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; dimethyl sulfoxide / 20 °C
With
copper(ll) sulfate pentahydrate; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; benzotriazol-1-ol; sodium L-ascorbate; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid;
In
dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;
4: Huisgen 1,3-dipolar cycloaddition;
DOI:10.1039/c2ob25428j