C₂₃H₃₈O₃Si

Base Information

Chemical Name:C₂₃H₃₈O₃Si
CAS No.:1423021-30-0
Molecular Formula:C₂₃H₃₈O₃Si
Molecular Weight:390.638
Hs Code.:

C<sub>23</sub>H<sub>38</sub>O<sub>3</sub>Si

Synonyms:C₂₃H₃₈O₃Si

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Chemical Property of C₂₃H₃₈O₃Si

Chemical Property:

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Technology Process of C₂₃H₃₈O₃Si

There total 9 articles about C₂₃H₃₈O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1423021-28-6
C₂₄H₃₇F₃O₆SSi

: 1423021-30-0
C₂₃H₃₈O₃Si

Guidance literature:: With tri-n-butyl-tin hydride; palladium diacetate; triphenylphosphine; In tetrahydrofuran; at 20 ℃; Inert atmosphere;
DOI:10.1002/cjoc.201201039

Reference yield:

: 2244-16-8,6485-40-1
(S)-p-mentha-6,8-dien-2-one

: 1423021-30-0
C₂₃H₃₈O₃Si

Guidance literature:: Multi-step reaction with 9 steps

1.1: dihydrogen peroxide; sodium hydroxide / methanol / 0 °C / Inert atmosphere

1.2: 0 °C / Inert atmosphere

2.1: 2,6-dimethylpyridine / dichloromethane / 20 °C / Inert atmosphere

3.1: methanol; diethyl ether / 0 °C / Inert atmosphere

4.1: lithium aluminium tetrahydride / tetrahydrofuran / Inert atmosphere

5.1: sodium hydride; tetra-(n-butyl)ammonium iodide / tetrahydrofuran / Inert atmosphere

6.1: potassium osmate(VI) dihydrate; 4-methylmorpholine N-oxide / Inert atmosphere

7.1: sodium periodate / water; acetone / 20 °C / Inert atmosphere

8.1: lithium hexamethyldisilazane / tetrahydrofuran / 3 h / -78 °C / Inert atmosphere

8.2: Inert atmosphere

9.1: palladium diacetate; triphenylphosphine; tri-n-butyl-tin hydride / tetrahydrofuran / 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; potassium osmate(VI) dihydrate; sodium periodate; lithium aluminium tetrahydride; dihydrogen peroxide; tri-n-butyl-tin hydride; palladium diacetate; tetra-(n-butyl)ammonium iodide; sodium hydride; 4-methylmorpholine N-oxide; triphenylphosphine; sodium hydroxide; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; acetone;
DOI:10.1002/cjoc.201201039

Reference yield:

(2R,3S,5S)-2-Chloro-3-hydroxy-5-isopropenyl-2-methyl-cyclohexanone: 156714-47-5
(2R,3S,5S)-2-Chloro-3-hydroxy-5-isopropenyl-2-methyl-cyclohexanone

: 1423021-30-0
C₂₃H₃₈O₃Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: 2,6-dimethylpyridine / dichloromethane / 20 °C / Inert atmosphere

2.1: methanol; diethyl ether / 0 °C / Inert atmosphere

3.1: lithium aluminium tetrahydride / tetrahydrofuran / Inert atmosphere

4.1: sodium hydride; tetra-(n-butyl)ammonium iodide / tetrahydrofuran / Inert atmosphere

5.1: potassium osmate(VI) dihydrate; 4-methylmorpholine N-oxide / Inert atmosphere

6.1: sodium periodate / water; acetone / 20 °C / Inert atmosphere

7.1: lithium hexamethyldisilazane / tetrahydrofuran / 3 h / -78 °C / Inert atmosphere

7.2: Inert atmosphere

8.1: palladium diacetate; triphenylphosphine; tri-n-butyl-tin hydride / tetrahydrofuran / 20 °C / Inert atmosphere

With 2,6-dimethylpyridine; potassium osmate(VI) dihydrate; sodium periodate; lithium aluminium tetrahydride; tri-n-butyl-tin hydride; palladium diacetate; tetra-(n-butyl)ammonium iodide; sodium hydride; 4-methylmorpholine N-oxide; triphenylphosphine; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; acetone;
DOI:10.1002/cjoc.201201039