4-carboxamido-5-(4-sec-butyl-2-aminoanilino)-1,2,3-triazole

Base Information

Chemical Name:4-carboxamido-5-(4-sec-butyl-2-aminoanilino)-1,2,3-triazole
CAS No.:304874-20-2
Molecular Formula:C₁₃H₁₈N₆O
Molecular Weight:274.326
Hs Code.:

Synonyms:4-carboxamido-5-(4-sec-butyl-2-aminoanilino)-1,2,3-triazole

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Chemical Property of 4-carboxamido-5-(4-sec-butyl-2-aminoanilino)-1,2,3-triazole

Chemical Property:

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Technology Process of 4-carboxamido-5-(4-sec-butyl-2-aminoanilino)-1,2,3-triazole

There total 6 articles about 4-carboxamido-5-(4-sec-butyl-2-aminoanilino)-1,2,3-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 304874-14-4
5-(4-sec-butyl-2-nitro-phenylamino)-1H-[1,2,3]triazole-4-carboxylic acid amide

: 304874-20-2
4-carboxamido-5-(4-sec-butyl-2-aminoanilino)-1,2,3-triazole

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; at 20 ℃; under 760 Torr;
DOI:10.1016/S0223-5234(00)00180-X

Reference yield:

: 20331-25-3
N-<4-(1-methylpropyl)phenyl>acetamide

: 304874-20-2
4-carboxamido-5-(4-sec-butyl-2-aminoanilino)-1,2,3-triazole

Guidance literature:: Multi-step reaction with 6 steps

1.1: 72 percent / fum. HNO₃ / acetic acid / 6 h / 50 °C

2.1: 92 percent / aq. H₂SO₄ / Heating

3.1: aq. HCl; NaNO₂ / 0 - 5 °C

3.2: NaN₃ / H₂O / 1 h / 0 - 5 °C

4.1: NaOEt / ethanol

4.2: ethanol / -10 - 20 °C

5.1: aq. NaOH / Heating

6.1: 91 percent / H₂ / 10 percent Pd/C / methanol / 20 °C / 760 Torr

With hydrogenchloride; sodium hydroxide; sulfuric acid; hydrogen; nitric acid; sodium ethanolate; sodium nitrite; palladium on activated charcoal; In methanol; ethanol; acetic acid; 1.1: Nitration / 2.1: Hydrolysis / 3.1: Diazotization / 3.2: Substitution / 4.1: Addition / 4.2: Cycloaddition / 5.1: Dimroth rearrangement / 6.1: Catalytic hydrogenation;
DOI:10.1016/S0223-5234(00)00180-X

Reference yield:

: 65439-19-2
4-sec-butyl-2-nitro-acetanilide

: 304874-20-2
4-carboxamido-5-(4-sec-butyl-2-aminoanilino)-1,2,3-triazole

Guidance literature:: Multi-step reaction with 5 steps

1.1: 92 percent / aq. H₂SO₄ / Heating

2.1: aq. HCl; NaNO₂ / 0 - 5 °C

2.2: NaN₃ / H₂O / 1 h / 0 - 5 °C

3.1: NaOEt / ethanol

3.2: ethanol / -10 - 20 °C

4.1: aq. NaOH / Heating

5.1: 91 percent / H₂ / 10 percent Pd/C / methanol / 20 °C / 760 Torr

With hydrogenchloride; sodium hydroxide; sulfuric acid; hydrogen; sodium ethanolate; sodium nitrite; palladium on activated charcoal; In methanol; ethanol; 1.1: Hydrolysis / 2.1: Diazotization / 2.2: Substitution / 3.1: Addition / 3.2: Cycloaddition / 4.1: Dimroth rearrangement / 5.1: Catalytic hydrogenation;
DOI:10.1016/S0223-5234(00)00180-X