2-<4-(Dimethylamino)phenylcarbonyloxymethyl>-3-methylbenzofuran

Base Information

• Chemical Name: 2-<4-(Dimethylamino)phenylcarbonyloxymethyl>-3-methylbenzofuran
• CAS No.: 128753-78-6
• Molecular Formula: C₁₉H₁₉NO₃
• Molecular Weight: 309.365
• Mol file: 128753-78-6.mol

Synonyms:2-<4-(Dimethylamino)phenylcarbonyloxymethyl>-3-methylbenzofuran

Chemical Property of 2-<4-(Dimethylamino)phenylcarbonyloxymethyl>-3-methylbenzofuran

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 2-<4-(Dimethylamino)phenylcarbonyloxymethyl>-3-methylbenzofuran

There total 1 articles about 2-<4-(Dimethylamino)phenylcarbonyloxymethyl>-3-methylbenzofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

2-(hydroxymethyl)-3-methylbenzofuran (55581-62-9) + p-N,N-dimethylaminobenzoic acid (619-84-1) → 2-<4-(Dimethylamino)phenylcarbonyloxymethyl>-3-methylbenzofuran (128753-78-6)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In dichloromethane; for 3h; Ambient temperature;

Reference yield: 25.0%

2-<4-(Dimethylamino)phenylcarbonyloxymethyl>-3-methylbenzofuran (128753-78-6) → 2a-<4-(Dimethylamino)phenylcarbonyloxymethyl>2a,7b-dihydro-3-methyl-1,2-dioxeto<3,4-b>benzofuran (128753-98-0)

Guidance literature:

With oxygen; 5,15,10,20-tetraphenylporphyrin; In dichloromethane; at -20 ℃; for 6h; Irradiation;

upstream raw materials:

2-(hydroxymethyl)-3-methylbenzofuran

p-N,N-dimethylaminobenzoic acid

Downstream raw materials:

2a-<4-(Dimethylamino)phenylcarbonyloxymethyl>2a,7b-dihydro-3-methyl-1,2-dioxeto<3,4-b>benzofuran