(Z)-S-(3-(hydroxymethyl)-5-phenylpent-2-en-1-yl) O,O-dimethyl phosphorodithioate

Base Information

Chemical Name:(Z)-S-(3-(hydroxymethyl)-5-phenylpent-2-en-1-yl) O,O-dimethyl phosphorodithioate
CAS No.:1610376-68-5
Molecular Formula:C₁₄H₂₁O₃PS₂
Molecular Weight:332.425
Hs Code.:

Synonyms:(Z)-S-(3-(hydroxymethyl)-5-phenylpent-2-en-1-yl) O,O-dimethyl phosphorodithioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-S-(3-(hydroxymethyl)-5-phenylpent-2-en-1-yl) O,O-dimethyl phosphorodithioate

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Technology Process of (Z)-S-(3-(hydroxymethyl)-5-phenylpent-2-en-1-yl) O,O-dimethyl phosphorodithioate

There total 3 articles about (Z)-S-(3-(hydroxymethyl)-5-phenylpent-2-en-1-yl) O,O-dimethyl phosphorodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1610376-65-2
2-phenethyl-2-vinyloxirane

: 756-80-9
O,O-dimethyl phosphorodithioic acid

: 1610376-68-5
(Z)-S-(3-(hydroxymethyl)-5-phenylpent-2-en-1-yl) O,O-dimethyl phosphorodithioate

: 1610376-71-0
(E)-S-(3-(hydroxymethyl)-5-phenylpent-2-en-1-yl) O,O-dimethyl phosphorodithioate

Guidance literature:: In toluene; at 20 ℃; for 5h; stereoselective reaction; Inert atmosphere;
DOI:10.1016/j.tetlet.2014.04.028

Reference yield:

: 1610376-87-8
C₁₂H₁₅ClO

: 1610376-68-5
(Z)-S-(3-(hydroxymethyl)-5-phenylpent-2-en-1-yl) O,O-dimethyl phosphorodithioate

: 1610376-71-0
(E)-S-(3-(hydroxymethyl)-5-phenylpent-2-en-1-yl) O,O-dimethyl phosphorodithioate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / mineral oil; dimethyl sulfoxide / 20 °C / Inert atmosphere

2: toluene / 5 h / 20 °C / Inert atmosphere

With sodium hydride; In dimethyl sulfoxide; toluene; mineral oil;
DOI:10.1016/j.tetlet.2014.04.028

Reference yield:

: 53931-59-2
5-phenyl-1-penten-3-one

: 1610376-68-5
(Z)-S-(3-(hydroxymethyl)-5-phenylpent-2-en-1-yl) O,O-dimethyl phosphorodithioate

: 1610376-71-0
(E)-S-(3-(hydroxymethyl)-5-phenylpent-2-en-1-yl) O,O-dimethyl phosphorodithioate

Guidance literature:: Multi-step reaction with 3 steps

1: n-butyllithium / tetrahydrofuran; diethyl ether / 0.37 h / -100 °C / Inert atmosphere

2: sodium hydride / mineral oil; dimethyl sulfoxide / 20 °C / Inert atmosphere

3: toluene / 5 h / 20 °C / Inert atmosphere

With n-butyllithium; sodium hydride; In tetrahydrofuran; diethyl ether; dimethyl sulfoxide; toluene; mineral oil;
DOI:10.1016/j.tetlet.2014.04.028