methyl 3-acetamido-4-O-benzoyl-2,3,6-trideoxy-2-fluoro-β-L-mannopyranoside

Base Information

Chemical Name:methyl 3-acetamido-4-O-benzoyl-2,3,6-trideoxy-2-fluoro-β-L-mannopyranoside
CAS No.:105600-40-6
Molecular Formula:C₁₆H₂₀FNO₅
Molecular Weight:325.337
Hs Code.:

Synonyms:methyl 3-acetamido-4-O-benzoyl-2,3,6-trideoxy-2-fluoro-β-L-mannopyranoside

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Chemical Property of methyl 3-acetamido-4-O-benzoyl-2,3,6-trideoxy-2-fluoro-β-L-mannopyranoside

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Technology Process of methyl 3-acetamido-4-O-benzoyl-2,3,6-trideoxy-2-fluoro-β-L-mannopyranoside

There total 4 articles about methyl 3-acetamido-4-O-benzoyl-2,3,6-trideoxy-2-fluoro-β-L-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 108-24-7
acetic anhydride

: 105600-39-3
methyl 3-azido-4-O-benzoyl-2,3,6-trideoxy-2-fluoro-β-L-lyxo-hex-5-enopyranoside

: 105600-40-6
methyl 3-acetamido-4-O-benzoyl-2,3,6-trideoxy-2-fluoro-β-L-mannopyranoside

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 12h;
DOI:10.1016/S0008-6215(00)90313-6

Reference yield:

: 3673-00-5
methyl 3-azido-4,6-O-benzylidene-3-deoxy-α-D-idopyranoside

: 105600-40-6
methyl 3-acetamido-4-O-benzoyl-2,3,6-trideoxy-2-fluoro-β-L-mannopyranoside

Guidance literature:: Multi-step reaction with 5 steps

1: 82 percent / pyridine / 2 h / 0 °C

2: 78 percent / tetrabutylammonium fluoride / dimethylformamide / 5 h / Ambient temperature

3: 56 percent / N-bromosuccinimide, BaCO₃ / CCl₄ / 1 h / Heating

4: 72 percent / silver fluoride / pyridine / 12 h / Ambient temperature

5: 60 percent / H₂ / 10percent Pd/C / methanol / 12 h

With pyridine; N-Bromosuccinimide; tetrabutyl ammonium fluoride; hydrogen; silver fluoride; barium carbonate; palladium on activated charcoal; In pyridine; methanol; tetrachloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0008-6215(00)90313-6

Reference yield:

: 105600-37-1
methyl 3-azido-4,6-O-benzylidene-2,3-dideoxy-2-fluoro-α-D-gulopyranoside

: 105600-40-6
methyl 3-acetamido-4-O-benzoyl-2,3,6-trideoxy-2-fluoro-β-L-mannopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 56 percent / N-bromosuccinimide, BaCO₃ / CCl₄ / 1 h / Heating

2: 72 percent / silver fluoride / pyridine / 12 h / Ambient temperature

3: 60 percent / H₂ / 10percent Pd/C / methanol / 12 h

With N-Bromosuccinimide; hydrogen; silver fluoride; barium carbonate; palladium on activated charcoal; In pyridine; methanol; tetrachloromethane;
DOI:10.1016/S0008-6215(00)90313-6