C₂₂H₂₅NO₃S

Base Information

Chemical Name:C₂₂H₂₅NO₃S
CAS No.:123836-50-0
Molecular Formula:C₂₂H₂₅NO₃S
Molecular Weight:383.511
Hs Code.:

C<sub>22</sub>H<sub>25</sub>NO<sub>3</sub>S

Synonyms:C₂₂H₂₅NO₃S

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Chemical Property of C₂₂H₂₅NO₃S

Chemical Property:

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Technology Process of C₂₂H₂₅NO₃S

There total 6 articles about C₂₂H₂₅NO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 19740-90-0,57378-34-4,65207-47-8,73176-71-3,73176-86-0,117468-08-3,637-90-1
(Z)-9-oxabicyclo[6.1.0]non-4-ene

: 123836-50-0
C₂₂H₂₅NO₃S

Guidance literature:: Multi-step reaction with 5 steps

1: 43 percent / boron trifluoride etherate / cyclohexane; diethyl ether; tetrahydrofuran / 0.17 h / -78 °C

2: 76 percent / Jones' reagent (chromium trioxide, sulfuric acid) / acetone / 0.25 h / 0 °C

3: 1.) lithium diisopropylamide / 1.) hexane, THF, -78 deg C, 30 min, 2.) a.) -78 deg C, 1 h, b.) from -78 deg C to RT, 1 h

4: 57 percent / 1.) sodium acetate, hydroxylamine hydrochloride, 2.) sodium bicarbonate, hydroxylamine hydrochloride / methanol / 80 °C / 1.) overnight, 2.) 36 h

5: pyridine / CH₂Cl₂ / Ambient temperature

With pyridine; Jones' reagent (chromium trioxide, sulfuric acid); boron trifluoride diethyl etherate; hydroxylamine hydrochloride; sodium acetate; sodium hydrogencarbonate; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; cyclohexane; acetone;

Reference yield:

: 123836-24-8
(+/-)-trans-8-phenyl-4-cycloocten-1-ol

: 123836-50-0
C₂₂H₂₅NO₃S

Guidance literature:: Multi-step reaction with 4 steps

1: 76 percent / Jones' reagent (chromium trioxide, sulfuric acid) / acetone / 0.25 h / 0 °C

2: 1.) lithium diisopropylamide / 1.) hexane, THF, -78 deg C, 30 min, 2.) a.) -78 deg C, 1 h, b.) from -78 deg C to RT, 1 h

3: 57 percent / 1.) sodium acetate, hydroxylamine hydrochloride, 2.) sodium bicarbonate, hydroxylamine hydrochloride / methanol / 80 °C / 1.) overnight, 2.) 36 h

4: pyridine / CH₂Cl₂ / Ambient temperature

With pyridine; Jones' reagent (chromium trioxide, sulfuric acid); hydroxylamine hydrochloride; sodium acetate; sodium hydrogencarbonate; lithium diisopropyl amide; In methanol; dichloromethane; acetone;

Reference yield:

: 123836-25-9
(+/-)-8-phenyl-4-cycloocten-1-one

: 123836-50-0
C₂₂H₂₅NO₃S

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) lithium diisopropylamide / 1.) hexane, THF, -78 deg C, 30 min, 2.) a.) -78 deg C, 1 h, b.) from -78 deg C to RT, 1 h

2: 57 percent / 1.) sodium acetate, hydroxylamine hydrochloride, 2.) sodium bicarbonate, hydroxylamine hydrochloride / methanol / 80 °C / 1.) overnight, 2.) 36 h

3: pyridine / CH₂Cl₂ / Ambient temperature

With pyridine; hydroxylamine hydrochloride; sodium acetate; sodium hydrogencarbonate; lithium diisopropyl amide; In methanol; dichloromethane;