C₂₃H₃₄N₆O₆

Base Information

Chemical Name:C₂₃H₃₄N₆O₆
CAS No.:1295471-65-6
Molecular Formula:C₂₃H₃₄N₆O₆
Molecular Weight:490.56
Hs Code.:

C<sub>23</sub>H<sub>34</sub>N<sub>6</sub>O<sub>6</sub>

Synonyms:C₂₃H₃₄N₆O₆

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Chemical Property of C₂₃H₃₄N₆O₆

Chemical Property:

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Technology Process of C₂₃H₃₄N₆O₆

There total 35 articles about C₂₃H₃₄N₆O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₄H₃₈N₆O₇

: 1295471-65-6
C₂₃H₃₄N₆O₆

Guidance literature:: With sodium periodate; In tetrahydrofuran; water; at 20 ℃; for 3h;
DOI:10.1002/anie.201008079

Reference yield:

: 1295471-59-8
C₁₇H₂₂N₄O₆

: 1295471-65-6
C₂₃H₃₄N₆O₆

Guidance literature:: Multi-step reaction with 11 steps

1: dmap; triethylamine / dichloromethane / 4 h / 0 - 20 °C

2: pyridine; trifluoromethylsulfonic anhydride / dichloromethane / 1 h / -78 - 0 °C / Inert atmosphere

3: ytterbium(III) triflate / toluene / 9 h / 20 - 80 °C

4: hydrogenchloride; water / tetrahydrofuran / 14 h / 0 - 20 °C

5: tris(dimethylamino)sulfonium trimethylsilyldifluoride / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

6: CSA / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

7: pyrographite; triethylamine / tetrahydrofuran / 0.25 h / -46 °C / Inert atmosphere

8: -46 - 20 °C

9: diisobutylaluminium hydride / dichloromethane; toluene / 1.5 h / -78 °C / Inert atmosphere

10: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water; acetone / 2 h / 20 °C

11: sodium periodate / tetrahydrofuran; water / 3 h / 20 °C

With pyridine; hydrogenchloride; dmap; sodium periodate; osmium(VIII) oxide; trifluoromethylsulfonic anhydride; tris(dimethylamino)sulfonium trimethylsilyldifluoride; water; diisobutylaluminium hydride; pyrographite; 4-methylmorpholine N-oxide; triethylamine; ytterbium(III) triflate; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1002/anie.201008079

Reference yield:

: 1295471-56-5
C₁₇H₂₀N₄O₅

: 1295471-65-6
C₂₃H₃₄N₆O₆

Guidance literature:: Multi-step reaction with 12 steps

1.1: zinc trifluoromethanesulfonate; acetic acid / 48 h / 80 °C

1.2: 1 h / 0 - 20 °C

2.1: dmap; triethylamine / dichloromethane / 4 h / 0 - 20 °C

3.1: pyridine; trifluoromethylsulfonic anhydride / dichloromethane / 1 h / -78 - 0 °C / Inert atmosphere

4.1: ytterbium(III) triflate / toluene / 9 h / 20 - 80 °C

5.1: hydrogenchloride; water / tetrahydrofuran / 14 h / 0 - 20 °C

6.1: tris(dimethylamino)sulfonium trimethylsilyldifluoride / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

7.1: CSA / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

8.1: pyrographite; triethylamine / tetrahydrofuran / 0.25 h / -46 °C / Inert atmosphere

9.1: -46 - 20 °C

10.1: diisobutylaluminium hydride / dichloromethane; toluene / 1.5 h / -78 °C / Inert atmosphere

11.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water; acetone / 2 h / 20 °C

12.1: sodium periodate / tetrahydrofuran; water / 3 h / 20 °C

With pyridine; hydrogenchloride; dmap; sodium periodate; osmium(VIII) oxide; trifluoromethylsulfonic anhydride; tris(dimethylamino)sulfonium trimethylsilyldifluoride; water; zinc trifluoromethanesulfonate; diisobutylaluminium hydride; pyrographite; acetic acid; 4-methylmorpholine N-oxide; triethylamine; ytterbium(III) triflate; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1002/anie.201008079