Technology Process of C26H32N4O5S2
There total 11 articles about C26H32N4O5S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: H2, water / 5percent Pd/C / tetrahydrofuran / 10 h / Ambient temperature
2: triethylamine / ethanol / 50 h / 0 °C
3: 75 percent / PCl5, 4-(dimethylamino)pyridine / CH2Cl2 / 12 h / Ambient temperature
4: K2CO3 / dimethylformamide / 45 h / 20 - 25 °C
5: conc. HCl / ethanol / 2 h / Heating
6: K2CO3 / acetone / 2 h / Heating
With
hydrogenchloride; dmap; phosphorus pentachloride; water; hydrogen; potassium carbonate; triethylamine;
palladium on activated charcoal;
In
tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; acetone;
DOI:10.1021/jm00013a013
- Guidance literature:
-
Multi-step reaction with 5 steps
1: triethylamine / ethanol / 50 h / 0 °C
2: 75 percent / PCl5, 4-(dimethylamino)pyridine / CH2Cl2 / 12 h / Ambient temperature
3: K2CO3 / dimethylformamide / 45 h / 20 - 25 °C
4: conc. HCl / ethanol / 2 h / Heating
5: K2CO3 / acetone / 2 h / Heating
With
hydrogenchloride; dmap; phosphorus pentachloride; potassium carbonate; triethylamine;
In
ethanol; dichloromethane; N,N-dimethyl-formamide; acetone;
DOI:10.1021/jm00013a013
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 93 percent / aq. Na2CO3, triphenylphosphine, palladium acetate / ethanol; toluene / 4 h / Heating
2: 64 percent / N-bromosuccinimide, benzoyl peroxide / chlorobenzene / 1 h / 120 °C
3: K2CO3 / dimethylformamide / 45 h / 20 - 25 °C
4: conc. HCl / ethanol / 2 h / Heating
5: K2CO3 / acetone / 2 h / Heating
With
hydrogenchloride; N-Bromosuccinimide; Perbenzoic acid; palladium diacetate; sodium carbonate; potassium carbonate; triphenylphosphine;
In
ethanol; N,N-dimethyl-formamide; chlorobenzene; acetone; toluene;
DOI:10.1021/jm00013a013