N-(2,3,4,6-tetra-O-pivaloyl-β-D-glucopyranosyl)-1-(4-chlorophenyl)-3-phenylprop-2-ynylamine

Base Information

Chemical Name:N-(2,3,4,6-tetra-O-pivaloyl-β-D-glucopyranosyl)-1-(4-chlorophenyl)-3-phenylprop-2-ynylamine
CAS No.:1164140-13-9
Molecular Formula:C₄₁H₅₄ClNO₉
Molecular Weight:740.334
Hs Code.:

Synonyms:N-(2,3,4,6-tetra-O-pivaloyl-β-D-glucopyranosyl)-1-(4-chlorophenyl)-3-phenylprop-2-ynylamine

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Chemical Property of N-(2,3,4,6-tetra-O-pivaloyl-β-D-glucopyranosyl)-1-(4-chlorophenyl)-3-phenylprop-2-ynylamine

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Technology Process of N-(2,3,4,6-tetra-O-pivaloyl-β-D-glucopyranosyl)-1-(4-chlorophenyl)-3-phenylprop-2-ynylamine

There total 2 articles about N-(2,3,4,6-tetra-O-pivaloyl-β-D-glucopyranosyl)-1-(4-chlorophenyl)-3-phenylprop-2-ynylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 536-74-3
phenylacetylene

: 856214-68-1
4-chloro-N-(2,3,4,6-tetra-O-pivaloyl-D-glucopyranosyl)benzylideneamine

: 1164140-13-9
N-(2,3,4,6-tetra-O-pivaloyl-β-D-glucopyranosyl)-1-(4-chlorophenyl)-3-phenylprop-2-ynylamine

Guidance literature:: 4-chloro-N-(2,3,4,6-tetra-O-pivaloyl-D-glucopyranosyl)benzylideneamine; With copper(I) triflate benzene complex; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;

phenylacetylene; In dichloromethane; at 20 ℃; for 24h; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1016/j.tetasy.2009.02.056

Reference yield:

: 536-74-3
phenylacetylene

: 856214-68-1
4-chloro-N-(2,3,4,6-tetra-O-pivaloyl-D-glucopyranosyl)benzylideneamine

: C₄₁H₅₄ClNO₉

: 1164140-13-9
N-(2,3,4,6-tetra-O-pivaloyl-β-D-glucopyranosyl)-1-(4-chlorophenyl)-3-phenylprop-2-ynylamine

Guidance literature:: 4-chloro-N-(2,3,4,6-tetra-O-pivaloyl-D-glucopyranosyl)benzylideneamine; With copper(II) bis(trifluoromethanesulfonate); In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;

phenylacetylene; In dichloromethane; at 20 ℃; for 32h; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1016/j.tetasy.2009.02.056