2-(trimethylsilyl)ethyl 3-[[3-[(8S,8aR)-1,3,4,7,8,8a-hexahydro-8-methyl-7-oxo-2H-2,4a-ethanonaphthalen-8-yl]-1-oxopropyl]amino]-2,4-dihydroxybenzoate

Base Information

Chemical Name:2-(trimethylsilyl)ethyl 3-[[3-[(8S,8aR)-1,3,4,7,8,8a-hexahydro-8-methyl-7-oxo-2H-2,4a-ethanonaphthalen-8-yl]-1-oxopropyl]amino]-2,4-dihydroxybenzoate
CAS No.:1195790-00-1
Molecular Formula:C₂₈H₃₉NO₆Si
Molecular Weight:513.706
Hs Code.:

Synonyms:2-(trimethylsilyl)ethyl 3-[[3-[(8S,8aR)-1,3,4,7,8,8a-hexahydro-8-methyl-7-oxo-2H-2,4a-ethanonaphthalen-8-yl]-1-oxopropyl]amino]-2,4-dihydroxybenzoate

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Chemical Property of 2-(trimethylsilyl)ethyl 3-[[3-[(8S,8aR)-1,3,4,7,8,8a-hexahydro-8-methyl-7-oxo-2H-2,4a-ethanonaphthalen-8-yl]-1-oxopropyl]amino]-2,4-dihydroxybenzoate

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Technology Process of 2-(trimethylsilyl)ethyl 3-[[3-[(8S,8aR)-1,3,4,7,8,8a-hexahydro-8-methyl-7-oxo-2H-2,4a-ethanonaphthalen-8-yl]-1-oxopropyl]amino]-2,4-dihydroxybenzoate

There total 1 articles about 2-(trimethylsilyl)ethyl 3-[[3-[(8S,8aR)-1,3,4,7,8,8a-hexahydro-8-methyl-7-oxo-2H-2,4a-ethanonaphthalen-8-yl]-1-oxopropyl]amino]-2,4-dihydroxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 1020070-44-3
2-(trimethylsilyl)-ethyl 3-amino-2,4-dihydroxybenzoate

: 1195789-99-1
(8S,8aR)-1,3,4,7,8,8a-hexahydro-8-methyl-7-oxo-2H-2,4a-ethanonaphthalene-8-propanoic acid

: 1195790-00-1
2-(trimethylsilyl)ethyl 3-[[3-[(8S,8aR)-1,3,4,7,8,8a-hexahydro-8-methyl-7-oxo-2H-2,4a-ethanonaphthalen-8-yl]-1-oxopropyl]amino]-2,4-dihydroxybenzoate

Guidance literature:: (8S,8aR)-1,3,4,7,8,8a-hexahydro-8-methyl-7-oxo-2H-2,4a-ethanonaphthalene-8-propanoic acid; With triethylamine; HATU; In N,N-dimethyl-formamide; at 23 ℃; for 0.166667h; Inert atmosphere;

2-(trimethylsilyl)-ethyl 3-amino-2,4-dihydroxybenzoate; In N,N-dimethyl-formamide; at 23 ℃; for 38h; Inert atmosphere;
DOI:10.1021/ol902194q

Reference yield: 56.0%

: 1195790-00-1
2-(trimethylsilyl)ethyl 3-[[3-[(8S,8aR)-1,3,4,7,8,8a-hexahydro-8-methyl-7-oxo-2H-2,4a-ethanonaphthalen-8-yl]-1-oxopropyl]amino]-2,4-dihydroxybenzoate

: 1195789-88-8
3-[[3-[(8S,8aR)-1,3,4,7,8,8a-hexahydro-8-methyl-7-oxo-2H-2,4a-ethanonaphthalen-8-yl]-1-oxopropyl]amino]-2,4-dihydroxybenzoic acid

Guidance literature:: With tris(dimethylamino)sulfonium trimethylsilyldifluoride; In N,N-dimethyl-formamide; at 40 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ol902194q