C₁₄H₂₃NOS

Base Information

• Chemical Name: C₁₄H₂₃NOS
• CAS No.: 1315613-42-3
• Molecular Formula: C₁₄H₂₃NOS
• Molecular Weight: 253.409

Synonyms:C₁₄H₂₃NOS

Chemical Property of C₁₄H₂₃NOS

Chemical Property:

Purity/Quality:

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Technology Process of C₁₄H₂₃NOS

There total 2 articles about C₁₄H₂₃NOS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C14H21NOS → C14H23NOS (1315613-42-3)

Guidance literature:

With [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; potassium tert-butylate; (1S,2R)-1-amino-2-indanol; isopropyl alcohol; at 40 ℃; for 3h; diastereoselective reaction; Inert atmosphere; Molecular sieve;

DOI:10.1021/jo101057s

Reference yield:

propiophenone (495-40-9) → C14H23NOS (1315613-42-3)

Guidance literature:

Multi-step reaction with 2 steps

1.1: titanium(IV) tetraethanolate / neat (no solvent) / 4 h / 72 °C / Inert atmosphere

2.1: 2-Amino-2-methyl-1-propanol; [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂ / isopropyl alcohol / 0.25 h / 50 °C / Inert atmosphere; Molecular sieve

2.2: 2 h / 50 °C / Inert atmosphere; Molecular sieve

With titanium(IV) tetraethanolate; [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; 2-Amino-2-methyl-1-propanol; In isopropyl alcohol;

DOI:10.15227/orgsyn.090.0338

Reference yield: 98.0%

C14H23NOS (1315613-42-3) → (R)-1-phenylbutylamine (2941-19-7,3789-60-4,6150-01-2,62311-56-2)

Guidance literature:

With hydrogenchloride; In methanol; diethyl ether; at 0 - 20 ℃; for 3h; Inert atmosphere;

DOI:10.15227/orgsyn.090.0338

upstream raw materials:

propiophenone

Downstream raw materials:

(R)-1-phenylbutylamine

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