C₂₃H₂₄N₂O₂

Base Information

Chemical Name:C₂₃H₂₄N₂O₂
CAS No.:1416772-49-0
Molecular Formula:C₂₃H₂₄N₂O₂
Molecular Weight:360.456
Hs Code.:

C<sub>23</sub>H<sub>24</sub>N<sub>2</sub>O<sub>2</sub>

Synonyms:C₂₃H₂₄N₂O₂

Suppliers and Price of C₂₃H₂₄N₂O₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₃H₂₄N₂O₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₃H₂₄N₂O₂

There total 5 articles about C₂₃H₂₄N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 95200-94-5
(S)-N-acetyl-(pyridin-3-yl)alanine methyl ester

: 1416772-49-0
C₂₃H₂₄N₂O₂

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / methanol / 18 h / 0 - 80 °C / Inert atmosphere; Schlenk technique

2: sodium cyanoborohydride; acetic acid / methanol / 24 h / 20 °C / Molecular sieve; Inert atmosphere; Schlenk technique

With thionyl chloride; sodium cyanoborohydride; acetic acid; In methanol;
DOI:10.1021/ml300385q

Reference yield:

: 500-22-1
3-pyridinecarboxaldehyde

: 1416772-49-0
C₂₃H₂₄N₂O₂

Guidance literature:: Multi-step reaction with 5 steps

1: sodium acetate; acetic anhydride / 18 h / 115 °C / Inert atmosphere; Schlenk technique

2: sodium acetate / 72 h / 20 °C / Inert atmosphere; Schlenk technique

3: tetrafluoroboric acid; (R,R)-(-)-1,2-bis[(o-methoxyphenyl)(phenyl) phosphino]ethane(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; hydrogen / methanol / 18 h / 50 °C / 3750.38 Torr / Autoclave; Schlenk technique

4: thionyl chloride / methanol / 18 h / 0 - 80 °C / Inert atmosphere; Schlenk technique

5: sodium cyanoborohydride; acetic acid / methanol / 24 h / 20 °C / Molecular sieve; Inert atmosphere; Schlenk technique

With tetrafluoroboric acid; thionyl chloride; (R,R)-(-)-1,2-bis[(o-methoxyphenyl)(phenyl) phosphino]ethane(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; hydrogen; sodium acetate; acetic anhydride; sodium cyanoborohydride; acetic acid; In methanol;
DOI:10.1021/ml300385q

Reference yield:

: 89890-92-6
N-acetyl-(β-3-pyridyl)-α,β-dehydroalanine

: 1416772-49-0
C₂₃H₂₄N₂O₂

Guidance literature:: Multi-step reaction with 4 steps

1: sodium acetate / 72 h / 20 °C / Inert atmosphere; Schlenk technique

2: tetrafluoroboric acid; (R,R)-(-)-1,2-bis[(o-methoxyphenyl)(phenyl) phosphino]ethane(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; hydrogen / methanol / 18 h / 50 °C / 3750.38 Torr / Autoclave; Schlenk technique

3: thionyl chloride / methanol / 18 h / 0 - 80 °C / Inert atmosphere; Schlenk technique

4: sodium cyanoborohydride; acetic acid / methanol / 24 h / 20 °C / Molecular sieve; Inert atmosphere; Schlenk technique

With tetrafluoroboric acid; thionyl chloride; (R,R)-(-)-1,2-bis[(o-methoxyphenyl)(phenyl) phosphino]ethane(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; hydrogen; sodium acetate; sodium cyanoborohydride; acetic acid; In methanol;
DOI:10.1021/ml300385q