Technology Process of trans,cis-(2,2'-bipyridyl)(PMe2Ph)2(CO)2rhenium(I) hexafluorophosphate
There total 1 articles about trans,cis-(2,2'-bipyridyl)(PMe2Ph)2(CO)2rhenium(I) hexafluorophosphate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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With
formic acid;
In
formic acid;
aq. formic acid; Re-complex was heated at reflux in 88% formic acid for 32 h under N2; cooled, solvent removed, dissolved in EtOH-acetone-water with added NH4PF6, solvent slowly removed in vac., chromd. (CH3CN-toluene, alumina); elem. anal.;