(C₆H₅)3(NH₂)C₂₇H₁₀N₄ONi

Base Information

• Chemical Name: (C₆H₅)3(NH₂)C₂₇H₁₀N₄ONi
• CAS No.: 437653-48-0
• Molecular Formula: C₄₅H₂₇N₅NiO
• Molecular Weight: 712.432

Synonyms:(C₆H₅)3(NH₂)C₂₇H₁₀N₄ONi

Chemical Property of (C₆H₅)3(NH₂)C₂₇H₁₀N₄ONi

Chemical Property:

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Technology Process of (C₆H₅)3(NH₂)C₂₇H₁₀N₄ONi

There total 2 articles about (C₆H₅)3(NH₂)C₂₇H₁₀N₄ONi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

bis(acetylacetonate)nickel(II) + (C6H5)3(NH2)C27H12N4O → (C6H5)3(NH2)C27H10N4ONi (437653-48-0)

Guidance literature:

In toluene; Ni compd. added to soln. of ligand (molar ratio 1:1) in toluene; heated at 80°C for 24 h; solvent evapd.; dissolved in CH2Cl2 and acetic acid; stirred at room temp. for 30 min; washed with satd. aq. NaHCO3 and water; dried (Na2SO4); filtered (silicagel, CH2Cl2); crystd. (CH2Cl2-MeOH); elem. anal.;

DOI:10.1021/ja017531n

Reference yield:

nickel(II) acetylacetonate + C45H29N5O → (C6H5)3(NH2)C27H10N4ONi (437653-48-0)

Guidance literature:

In toluene; equimol., refluxed;

DOI:10.1039/b008740h

Reference yield: 85.0%

bis(acetylacetonate)nickel(II) + (C6H5)3(NH2)C27H10N4ONi (437653-48-0) → ((C6H5)3(NH)C27H10N4O)2Ni3 (331717-01-2)

Guidance literature:

In toluene; soln. of Ni complex in toluene treated with Ni compd. (molar ratio 2:1) at 40°C for a few min; solvent evapd.; crystd. (CH2Cl2-MeOH); elem. anal.;

DOI:10.1021/ja017531n

Downstream raw materials:

((C₆H₅)3(NH)C₂₇H₁₀N₄O)2Ni₃

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