methyl 4-C-[(3R,4R,5S)-4-(2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-3-benzyloxy-5-benzyloxycarbonylpiperidin-1-ylmethyl]-3-O-benzyl-2-(benzyloxycarbonyl)-amino-2,4-dideoxy-α-D-glucopyranoside

Base Information

Chemical Name:methyl 4-C-[(3R,4R,5S)-4-(2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-3-benzyloxy-5-benzyloxycarbonylpiperidin-1-ylmethyl]-3-O-benzyl-2-(benzyloxycarbonyl)-amino-2,4-dideoxy-α-D-glucopyranoside
CAS No.:1248566-77-9
Molecular Formula:C₆₃H₇₁N₅O₁₄
Molecular Weight:1122.28
Hs Code.:

methyl 4-C-[(3R,4R,5S)-4-(2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-3-benzyloxy-5-benzyloxycarbonylpiperidin-1-ylmethyl]-3-O-benzyl-2-(benzyloxycarbonyl)-amino-2,4-dideoxy-α-D-glucopyranoside

Synonyms:methyl 4-C-[(3R,4R,5S)-4-(2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-3-benzyloxy-5-benzyloxycarbonylpiperidin-1-ylmethyl]-3-O-benzyl-2-(benzyloxycarbonyl)-amino-2,4-dideoxy-α-D-glucopyranoside

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Chemical Property of methyl 4-C-[(3R,4R,5S)-4-(2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-3-benzyloxy-5-benzyloxycarbonylpiperidin-1-ylmethyl]-3-O-benzyl-2-(benzyloxycarbonyl)-amino-2,4-dideoxy-α-D-glucopyranoside

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Technology Process of methyl 4-C-[(3R,4R,5S)-4-(2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-3-benzyloxy-5-benzyloxycarbonylpiperidin-1-ylmethyl]-3-O-benzyl-2-(benzyloxycarbonyl)-amino-2,4-dideoxy-α-D-glucopyranoside

There total 1 articles about methyl 4-C-[(3R,4R,5S)-4-(2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-3-benzyloxy-5-benzyloxycarbonylpiperidin-1-ylmethyl]-3-O-benzyl-2-(benzyloxycarbonyl)-amino-2,4-dideoxy-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1248566-76-8
C₆₉H₈₅N₅O₁₄Si

: 1248566-77-9
methyl 4-C-[(3R,4R,5S)-4-(2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-3-benzyloxy-5-benzyloxycarbonylpiperidin-1-ylmethyl]-3-O-benzyl-2-(benzyloxycarbonyl)-amino-2,4-dideoxy-α-D-glucopyranoside

Guidance literature:: With formic acid; In tetrahydrofuran; water; at 60 ℃; for 3h;
DOI:10.1016/j.carres.2010.05.032

Reference yield:

: 1248566-77-9
methyl 4-C-[(3R,4R,5S)-4-(2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-3-benzyloxy-5-benzyloxycarbonylpiperidin-1-ylmethyl]-3-O-benzyl-2-(benzyloxycarbonyl)-amino-2,4-dideoxy-α-D-glucopyranoside

: C₆₃H₇₁N₅O₂₀S₂*2H₃N

Guidance literature:: methyl 4-C-[(3R,4R,5S)-4-(2-azido-3,4-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-3-benzyloxy-5-benzyloxycarbonylpiperidin-1-ylmethyl]-3-O-benzyl-2-(benzyloxycarbonyl)-amino-2,4-dideoxy-α-D-glucopyranoside; With sulfur trioxide trimethylamine complex; In N,N-dimethyl-formamide; at 45 ℃; for 16h; Inert atmosphere;

With ammonium hydroxide; In methanol; dichloromethane; water;
DOI:10.1016/j.carres.2010.05.032