Technology Process of C43H45NO9
There total 3 articles about C43H45NO9 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
dichloromethane;
at 20 ℃;
for 24h;
Inert atmosphere;
DOI:10.1016/j.tet.2012.02.040
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 4-methyl-morpholine; isobutyl chloroformate / acetone / 2 h / -15 - 20 °C / Inert atmosphere
2: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 24 h / 20 °C / Inert atmosphere
With
4-methyl-morpholine; dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; isobutyl chloroformate;
In
dichloromethane; acetone;
DOI:10.1016/j.tet.2012.02.040
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dmap / tetrahydrofuran / 5 h / 50 °C / Inert atmosphere
2: 4-methyl-morpholine; isobutyl chloroformate / acetone / 2 h / -15 - 20 °C / Inert atmosphere
3: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 24 h / 20 °C / Inert atmosphere
With
4-methyl-morpholine; dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; isobutyl chloroformate;
In
tetrahydrofuran; dichloromethane; acetone;
DOI:10.1016/j.tet.2012.02.040