2-tert-Butyl-1-(4-nitrophenylhydrazono)-1H-isoindolium-tetrafluoroborat

Base Information

• Chemical Name: 2-tert-Butyl-1-(4-nitrophenylhydrazono)-1H-isoindolium-tetrafluoroborat
• CAS No.: 73286-85-8
• Molecular Formula: BF₄*C₁₈H₁₉N₄O₂
• Molecular Weight: 410.179

Synonyms:2-tert-Butyl-1-(4-nitrophenylhydrazono)-1H-isoindolium-tetrafluoroborat

Chemical Property of 2-tert-Butyl-1-(4-nitrophenylhydrazono)-1H-isoindolium-tetrafluoroborat

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Technology Process of 2-tert-Butyl-1-(4-nitrophenylhydrazono)-1H-isoindolium-tetrafluoroborat

There total 2 articles about 2-tert-Butyl-1-(4-nitrophenylhydrazono)-1H-isoindolium-tetrafluoroborat which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

2-tert-Butyl-2H-isoindol (55023-87-5) + 4-nitrobenzenediazonium tetrafluoroborate (456-27-9) → 2-tert-Butyl-1-(4-nitrophenylhydrazono)-1H-isoindolium-tetrafluoroborat (73286-85-8)

Guidance literature:

In acetone; at 0 ℃; for 2h;

Reference yield: 39.0%

4-nitrobenzenediazonium tetrafluoroborate (456-27-9) + 2-tert-Butyl-1-(4-chlorphenylazo)-2H-isoindol (73286-86-9) → 2-tert-Butyl-1-(4-nitrophenylhydrazono)-1H-isoindolium-tetrafluoroborat (73286-85-8)

Guidance literature:

In diethyl ether; acetone; Ambient temperature;

Reference yield: 98.0%

2-tert-Butyl-1-(4-nitrophenylhydrazono)-1H-isoindolium-tetrafluoroborat (73286-85-8) → 2-tert-Butyl-1-(4-nitrophenylazo)-2H-isoindol (73286-90-5)

Guidance literature:

With sodium hydroxide; In diethyl ether; for 2h; Ambient temperature;

upstream raw materials:

2-tert-Butyl-2H-isoindol

4-nitrobenzenediazonium tetrafluoroborate

2-tert-Butyl-1-(4-chlorphenylazo)-2H-isoindol

Downstream raw materials:

2-tert-Butyl-1-(4-nitrophenylazo)-2H-isoindol

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