1-[4-(2-cyclopropylethynyl)phenyl]-N-ethoxy-2-(1,2,4-triazol-1-yl)ethanimine

Base Information

Chemical Name:1-[4-(2-cyclopropylethynyl)phenyl]-N-ethoxy-2-(1,2,4-triazol-1-yl)ethanimine
CAS No.:1458957-97-5
Molecular Formula:C₁₇H₁₈N₄O
Molecular Weight:294.356
Hs Code.:

Synonyms:1-[4-(2-cyclopropylethynyl)phenyl]-N-ethoxy-2-(1,2,4-triazol-1-yl)ethanimine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-[4-(2-cyclopropylethynyl)phenyl]-N-ethoxy-2-(1,2,4-triazol-1-yl)ethanimine

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Technology Process of 1-[4-(2-cyclopropylethynyl)phenyl]-N-ethoxy-2-(1,2,4-triazol-1-yl)ethanimine

There total 3 articles about 1-[4-(2-cyclopropylethynyl)phenyl]-N-ethoxy-2-(1,2,4-triazol-1-yl)ethanimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6746-94-7
Cyclopropylacetylene

: 1-(4-bromophenyl)-N-ethoxy-2-(1,2,4-triazol-1-yl)ethanimine

: 1458957-97-5
1-[4-(2-cyclopropylethynyl)phenyl]-N-ethoxy-2-(1,2,4-triazol-1-yl)ethanimine

Guidance literature:: With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In N,N-dimethyl-formamide; at 120 ℃; for 1h; Inert atmosphere; Microwave irradiation;

Reference yield:

: 60850-59-1
1-(4-bromophenyl)-2-(1H-1,2,4-triazol-1-yl)-ethanone

: 1458957-97-5
1-[4-(2-cyclopropylethynyl)phenyl]-N-ethoxy-2-(1,2,4-triazol-1-yl)ethanimine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium acetate / ethanol / 95 °C / Sealed tube

2: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / N,N-dimethyl-formamide / 1 h / 120 °C / Inert atmosphere; Microwave irradiation

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium acetate; triethylamine; In ethanol; N,N-dimethyl-formamide;

Reference yield:

: 99-73-0,132309-76-3
para-bromophenacyl bromide

: 1458957-97-5
1-[4-(2-cyclopropylethynyl)phenyl]-N-ethoxy-2-(1,2,4-triazol-1-yl)ethanimine

Guidance literature:: Multi-step reaction with 3 steps

1: N,N-dimethyl-formamide / 1 h / 0 - 5 °C

2: sodium acetate / ethanol / 95 °C / Sealed tube

3: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / N,N-dimethyl-formamide / 1 h / 120 °C / Inert atmosphere; Microwave irradiation

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium acetate; triethylamine; In ethanol; N,N-dimethyl-formamide;