8-(N-Methyl-N-carbobenzoxy)methylaminoquinoline-5-carboxylic acid hydrazide

Base Information

Chemical Name:8-(N-Methyl-N-carbobenzoxy)methylaminoquinoline-5-carboxylic acid hydrazide
CAS No.:82967-26-8
Molecular Formula:C₂₀H₂₀N₄O₃
Molecular Weight:364.404
Hs Code.:

Synonyms:8-(N-Methyl-N-carbobenzoxy)methylaminoquinoline-5-carboxylic acid hydrazide

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Chemical Property of 8-(N-Methyl-N-carbobenzoxy)methylaminoquinoline-5-carboxylic acid hydrazide

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Technology Process of 8-(N-Methyl-N-carbobenzoxy)methylaminoquinoline-5-carboxylic acid hydrazide

There total 5 articles about 8-(N-Methyl-N-carbobenzoxy)methylaminoquinoline-5-carboxylic acid hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 82967-45-1
Ethyl 8-(N-methyl-N-carbobenzoxy)methylaminoquinoline-5-carboxylate

: 82967-26-8
8-(N-Methyl-N-carbobenzoxy)methylaminoquinoline-5-carboxylic acid hydrazide

Guidance literature:: With hydrazine hydrate; In ethanol; for 6h; Heating;
DOI:10.1007/BF00506150

Reference yield:

: 82967-39-3
Ethyl 8-methylquinoline-5-carboxylate

: 82967-26-8
8-(N-Methyl-N-carbobenzoxy)methylaminoquinoline-5-carboxylic acid hydrazide

Guidance literature:: Multi-step reaction with 4 steps

1: 75 percent / N-Bromosuccimide / Benzoyl peroxide / CCl₄ / Heating; Irradiation

2: 40 percent / methanol / 1.5 h

3: 56.6 percent / Magnesium oxide / CHCl₃; H₂O / 1.) 30 min, ice cooling, 2.) 1 h, 20 deg C_.

4: 80 percent / Hydrazine hydrate / ethanol / 6 h / Heating

With N-Bromosuccinimide; magnesium oxide; hydrazine hydrate; dibenzoyl peroxide; In methanol; tetrachloromethane; ethanol; chloroform; water;
DOI:10.1007/BF00506150

Reference yield:

: 74316-57-7
8-methylquinoline-5-carbonitrile

: 82967-26-8
8-(N-Methyl-N-carbobenzoxy)methylaminoquinoline-5-carboxylic acid hydrazide

Guidance literature:: Multi-step reaction with 5 steps

1: 48 percent / Conc_. sulfuric acid / 48 h / Heating

2: 75 percent / N-Bromosuccimide / Benzoyl peroxide / CCl₄ / Heating; Irradiation

3: 40 percent / methanol / 1.5 h

4: 56.6 percent / Magnesium oxide / CHCl₃; H₂O / 1.) 30 min, ice cooling, 2.) 1 h, 20 deg C_.

5: 80 percent / Hydrazine hydrate / ethanol / 6 h / Heating

With N-Bromosuccinimide; magnesium oxide; hydrazine hydrate; sulfuric acid; dibenzoyl peroxide; In methanol; tetrachloromethane; ethanol; chloroform; water;
DOI:10.1007/BF00506150