Technology Process of 8-(N-Methyl-N-carbobenzoxy)methylaminoquinoline-5-carboxylic acid hydrazide
There total 5 articles about 8-(N-Methyl-N-carbobenzoxy)methylaminoquinoline-5-carboxylic acid hydrazide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrazine hydrate;
In
ethanol;
for 6h;
Heating;
DOI:10.1007/BF00506150
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 75 percent / N-Bromosuccimide / Benzoyl peroxide / CCl4 / Heating; Irradiation
2: 40 percent / methanol / 1.5 h
3: 56.6 percent / Magnesium oxide / CHCl3; H2O / 1.) 30 min, ice cooling, 2.) 1 h, 20 deg C.
4: 80 percent / Hydrazine hydrate / ethanol / 6 h / Heating
With
N-Bromosuccinimide; magnesium oxide; hydrazine hydrate;
dibenzoyl peroxide;
In
methanol; tetrachloromethane; ethanol; chloroform; water;
DOI:10.1007/BF00506150
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 48 percent / Conc. sulfuric acid / 48 h / Heating
2: 75 percent / N-Bromosuccimide / Benzoyl peroxide / CCl4 / Heating; Irradiation
3: 40 percent / methanol / 1.5 h
4: 56.6 percent / Magnesium oxide / CHCl3; H2O / 1.) 30 min, ice cooling, 2.) 1 h, 20 deg C.
5: 80 percent / Hydrazine hydrate / ethanol / 6 h / Heating
With
N-Bromosuccinimide; magnesium oxide; hydrazine hydrate;
sulfuric acid; dibenzoyl peroxide;
In
methanol; tetrachloromethane; ethanol; chloroform; water;
DOI:10.1007/BF00506150
