(Ph₄P)2{Fe₄S₄(1,3,5-tris((4,6-dimethyl-3-mercaptophenyl)thio)-2,4,6-tris(p-tolylthio)benzene)Cl}

Base Information

• Chemical Name: (Ph₄P)2{Fe₄S₄(1,3,5-tris((4,6-dimethyl-3-mercaptophenyl)thio)-2,4,6-tris(p-tolylthio)benzene)Cl}
• CAS No.: 113087-96-0
• Molecular Formula: 2C₂₄H₂₀P*C₅₁H₄₅ClFe₄S₁₃
• Molecular Weight: 2012.41

Synonyms:(Ph₄P)2{Fe₄S₄(1,3,5-tris((4,6-dimethyl-3-mercaptophenyl)thio)-2,4,6-tris(p-tolylthio)benzene)Cl}

Chemical Property of (Ph₄P)2{Fe₄S₄(1,3,5-tris((4,6-dimethyl-3-mercaptophenyl)thio)-2,4,6-tris(p-tolylthio)benzene)Cl}

Chemical Property:

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Technology Process of (Ph₄P)2{Fe₄S₄(1,3,5-tris((4,6-dimethyl-3-mercaptophenyl)thio)-2,4,6-tris(p-tolylthio)benzene)Cl}

There total 5 articles about (Ph₄P)2{Fe₄S₄(1,3,5-tris((4,6-dimethyl-3-mercaptophenyl)thio)-2,4,6-tris(p-tolylthio)benzene)Cl} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

(Ph4P)2{Fe4S4(SEt)4} + 1,3,5-tris((4,6-dimethyl-3-mercaptophenyl)thio)-2,4,6-tris(p-tolylthio)benzene (107540-22-7) → (Ph4P)2{Fe4S4(1,3,5-tris((4,6-dimethyl-3-mercaptophenyl)thio)-2,4,6-tris(p-tolylthio)benzene)Cl} (113087-96-0)

Guidance literature:

With pivaloyl chloride; acetonitrile; In chloroform; N,N-dimethyl-formamide; (N2); stirred under dynamic vacuum for 1h; pivaloyl chloride was added; stirred for 30 min; acetonitrile was added to the filtrate; stored at -20°C; filtered; washed; in vacuo dried;

Reference yield: 58.0%

(Ph4P)2(Fe4S4(SEt)(1,3,5-tris((4,6-dimethyl-3-mercaptophenyl)thio)-2,4,6-tris(p-tolylthio)benzene)) (113087-95-9) → (Ph4P)2{Fe4S4(1,3,5-tris((4,6-dimethyl-3-mercaptophenyl)thio)-2,4,6-tris(p-tolylthio)benzene)Cl} (113087-96-0)

Guidance literature:

With pivaloyl chloride; In N,N-dimethyl-formamide; mixture stirred for 4 h and layered with ether; formation of an oil after 1 h; soln. decanted away from the oil; ether added to the removed soln.; crystalline material is formed after 1 d, collected, washed with acetonitrile and dried in vacuo; filtrate is treated similarily;

DOI:10.1021/ja00216a023

Reference yield:

Fe4S4C51H45S10(C6H3Cl2)(2-) (107556-53-6) → (Ph4P)2{Fe4S4(1,3,5-tris((4,6-dimethyl-3-mercaptophenyl)thio)-2,4,6-tris(p-tolylthio)benzene)Cl} (113087-96-0)

Guidance literature:

With t-C₄H₉COCl; In acetonitrile; reaction (1)H-NMR spectroscopically monitored; quantitative reaction;

DOI:10.1021/ja00216a023

upstream raw materials:

(Ph₄P)2(Fe₄S₄(SEt)(1,3,5-tris((4,6-dimethyl-3-mercaptophenyl)thio)-2,4,6-tris(p-tolylthio)benzene))

1,3,5-tris((4,6-dimethyl-3-mercaptophenyl)thio)-2,4,6-tris(p-tolylthio)benzene

Fe₄S₄C₅₁H₄₅S₁₀(C₆H₃Cl₂)^(2-)

Fe₄S₄C₅₁H₄₅S₁₀C₆H₄Br^(2-)

Downstream raw materials:

(Ph₄P)2(Fe₄S₄(SEt)(1,3,5-tris((4,6-dimethyl-3-mercaptophenyl)thio)-2,4,6-tris(p-tolylthio)benzene))

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