methyl 4-(2-((trans-4-(methoxycarbonyl)cyclohexyl)methyl)-2H-tetrazol-5-yl)-6-methylpicolinate

Base Information

• Chemical Name: methyl 4-(2-((trans-4-(methoxycarbonyl)cyclohexyl)methyl)-2H-tetrazol-5-yl)-6-methylpicolinate
• CAS No.: 1112182-58-7
• Molecular Formula: C₁₈H₂₃N₅O₄
• Molecular Weight: 373.412

Synonyms:methyl 4-(2-((trans-4-(methoxycarbonyl)cyclohexyl)methyl)-2H-tetrazol-5-yl)-6-methylpicolinate

Chemical Property of methyl 4-(2-((trans-4-(methoxycarbonyl)cyclohexyl)methyl)-2H-tetrazol-5-yl)-6-methylpicolinate

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Technology Process of methyl 4-(2-((trans-4-(methoxycarbonyl)cyclohexyl)methyl)-2H-tetrazol-5-yl)-6-methylpicolinate

There total 1 articles about methyl 4-(2-((trans-4-(methoxycarbonyl)cyclohexyl)methyl)-2H-tetrazol-5-yl)-6-methylpicolinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 6-methyl-4-(2H-tetrazol-5-yl)picolinate (890127-04-5) + C15H19NO7S (1112182-56-5) → methyl 4-(2-((trans-4-(methoxycarbonyl)cyclohexyl)methyl)-2H-tetrazol-5-yl)-6-methylpicolinate (1112182-58-7)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In acetonitrile;

DOI:10.1016/j.bmcl.2009.11.081

Reference yield: 80.0%

methyl 4-(2-((trans-4-(methoxycarbonyl)cyclohexyl)methyl)-2H-tetrazol-5-yl)-6-methylpicolinate (1112182-58-7) + 3-hydroxybenzylamine (73604-31-6) → methyl trans-4-((5-(2-((3-hydroxy-benzyl)carbamoyl)-6-methyl-pyridin-4-yl)-2H-tetrazol-2-yl)methyl)cyclohexanecarboxylate (1112172-86-7)

Guidance literature:

In methanol; at 60 ℃; for 96h;

Reference yield: 65.0%

methyl 4-(2-((trans-4-(methoxycarbonyl)cyclohexyl)methyl)-2H-tetrazol-5-yl)-6-methylpicolinate (1112182-58-7) + [3-(aminomethyl)phenyl]methanol (34231-22-6) → methyl trans-4-((5-(2-((3-(hydroxymethyl)benzyl)carbamoyl)-6-methylpyridin-4-yl)-2H-tetrazol-2-yl)methyl)cyclohexanecarboxylate (1112172-80-1)

Guidance literature:

In N,N-dimethyl-formamide; at 60 ℃; for 72h;

upstream raw materials:

methyl 6-methyl-4-(2H-tetrazol-5-yl)picolinate

C₁₅H₁₉NO₇S

Downstream raw materials:

methyl trans-4-((5-(2-((3-(hydroxymethyl)benzyl)carbamoyl)-6-methylpyridin-4-yl)-2H-tetrazol-2-yl)methyl)cyclohexanecarboxylate

methyl trans-4-((5-(2-((3-(difluoromethoxy)-benzyl)carbamoyl)-6-methyl-pyridin-4-yl)-2H-tetrazol-2-yl)methyl)cyclohexanecarboxylate

methyl trans-4-((5-(2-((3-hydroxy-benzyl)carbamoyl)-6-methyl-pyridin-4-yl)-2H-tetrazol-2-yl)methyl)cyclohexanecarboxylate

methyl trans-4-((5-(2-((3,4-difluoro-benzyl)carbamoyl)-6-methyl-pyridin-4-yl)-2H-tetrazol-2-yl)methyl)cyclohexanecarboxylate

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